3,3-二甲基-2,4-戊二酮合成路线 (共 46 条)
反应条件
platinum (IV)-chloride T=100°C; 2 h; other reagent, solvent, reaction time; Product distribution;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 32, p. 1217 - 1220
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 6 p. 1346 - 1350
反应条件
zuletzt unter Erwaermen, und Zersetzung mit Eis und verd.Saeure;
参考文献
Kohler, Erickson
Journal of the American Chemical Society, 1931 , vol. 53, p. 2301,2307
反应条件
sodium hydroxide; ethyl orthosilicate T=140°C; 24 h;
参考文献
Zhang, Wen; Leng, Xuebing; Sun, Wen-Hua
Journal of Chemical Research - Part S, 2003 , # 12 p. 808 - 809
反应条件
platinum (IV)-chloride T=100°C; 2 h; other reagent, solvent, reaction time; Product distribution;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 32, p. 1217 - 1220
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 6 p. 1346 - 1350
参考文献
Bromham; Pinder
Journal of the Chemical Society, 1959 , p. 2688,2693
反应条件
diethyl ether; nickel T=125°C; P=110326 - 147102 Torr; Hydrogenation;
参考文献
Sprague; Adkins
Journal of the American Chemical Society, 1934 , vol. 56, p. 2669,2671
反应条件
sodium acetate; acetic acid in ethanol 40 h; Heatingother 2,2-disubstituted 1,3-diketones; in absence of CH3COOH; var. time; Product distributionMechanism;
参考文献
Journal of Chemical Research, Miniprint, , # 10 p. 2401 - 2410
参考文献
Kohler, Erickson
Journal of the American Chemical Society, 1931 , vol. 53, p. 2301,2307
反应条件
hydroxylamine hydrochloride; potassium carbonate in water T=3 - 5°C; 12 h;
参考文献
Ershov, A. Yu.; Yakimovich, S. I.; Zelenin, K. N.; Zerova, I. V.
Journal of Organic Chemistry USSR (English Translation), 1988 , vol. 24, # 11 p. 2062 - 2070
Zhurnal Organicheskoi Khimii, 1988 , vol. 24, # 11 p. 2287 - 2297
反应条件
dihydrogen peroxide; copper(l) chloride in water; butanone; tert-butyl alcohol
T=20°C; 12 h; Acidic conditions;
参考文献
Dichtl, Alexander; Seyfried, Martin; Schoening, Kai-Uwe
Synlett, 2008 , # 12 p. 1877 - 1881