tetrabutyl ammonium fluoride in N,N-dimethyl-formamide T=20°C; Substitution; 3 h; UV-irradiation;

FeCl3·6H2O in 1,2-dichloro-ethane T=20 - 100°C; 12 h; Schlenk techniqueInert atmosphere;

ethanol T=100°C;

1: iron(II) chloride; di-tert-butyl peroxide / 8 h / 80 °C / |Inert atmosphere; |Schlenk technique 2: FeCl3·6H2O / 1,2-dichloro-ethane / 12 h / 20 - 100 °C / |Schlenk technique; |Inert atmosphere View Scheme

暂无反应条件数据