in toluene (N2); stirring a soln. of titanium complex and phosphite in toluene at 60°C for 1 h, cooling to 25°C; evapn., dissolving in pentane, filtration through Kieselgur, concn., crystn. at -30°C; elem. anal.;
参考文献
Meichel, E.; Stein, Th.; Kralik, J.; Rheinwald, G.; Lang, H.
Journal of Organometallic Chemistry, 2002 , vol. 649, # 2 p. 191 - 198
in toluene (N2); stirring a soln. of titanium complex and phosphite in toluene at 60°C for 1 h, cooling to 25°C; evapn., dissolving in pentane, filtration through Kieselgur, concn., crystn. at -30°C; elem. anal.;
参考文献
Meichel, E.; Stein, Th.; Kralik, J.; Rheinwald, G.; Lang, H.
Journal of Organometallic Chemistry, 2002 , vol. 649, # 2 p. 191 - 198
in dichloromethane all manipulations under N2 atm.; soln. of P and Pd compds. stirred for 1.5 h at room temp.; MeOH added, concd. in vac.; elem. anal.;
参考文献
Bedford, Robin B.; Betham, Michael; Coles, Simon J.; Horton, Peter N.; Lopez-Saez, Maria-Jose
Polyhedron, 2006 , vol. 25, # 4 p. 1003 - 1010
