Alpha-甲基苯乙酸甲酯合成路线 （共 146 条）
反应条件
3-chloro-benzenecarboperoxoic acid T=25°C; 5 h;
参考文献
Uemura, Sakae; Ohe, Kouichi; Yamauchi, Takayoshi; Mizutaki, Shoichi; Tamaki, Kentaro
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1990 , # 4 p. 907 - 910
参考文献
Ohmiya, Hirohisa; Makida, Yusuke; Li, Dong; Tanabe, Masahito; Sawamura, Masaya
Journal of the American Chemical Society, 2010 , vol. 132, # 2 p. 879 - 889
反应条件
1.1: tetrahydrofuran / -80 - 0 °C / Inert atmosphere 2.1: potassium fluoride / ethylene glycol dimethyl ether / 18 h / 20 °C / Inert atmosphere 3.1: chloro-trimethyl-silane / ethylene glycol dimethyl ether / 0.33 h / -20 - -10 °C / Inert atmosphere 3.2: 13 h / -20 - 20 °C / Inert atmosphere View Scheme
参考文献
Elkin, Pavel K.; Levin, Vitalij V.; Dilman, Alexander D.; Struchkova, Marina I.; Belyakov, Pavel A.; Arkhipov, Dmitry E.; Korlyukov, Alexander A.; Tartakovsky, Vladimir A.
Tetrahedron Letters, 2011 , vol. 52, # 41 p. 5259 - 5263
反应条件
1.1: trifluoroacetic acid / 0.25 h / 20 °C / Inert atmosphere 2.1: potassium fluoride / ethylene glycol dimethyl ether / 18 h / 20 °C / Inert atmosphere 3.1: chloro-trimethyl-silane / ethylene glycol dimethyl ether / 0.33 h / -20 - -10 °C / Inert atmosphere 3.2: 13 h / -20 - 20 °C / Inert atmosphere View Scheme
参考文献
Elkin, Pavel K.; Levin, Vitalij V.; Dilman, Alexander D.; Struchkova, Marina I.; Belyakov, Pavel A.; Arkhipov, Dmitry E.; Korlyukov, Alexander A.; Tartakovsky, Vladimir A.
Tetrahedron Letters, 2011 , vol. 52, # 41 p. 5259 - 5263
反应条件
in methanol 15 h; Irradiation;
参考文献
Bergmark, William R.; Barnes, Curtis; Clark, Jeffrey; Paparian, Seth; Marynowski, Susan
Journal of Organic Chemistry, 1985 , vol. 50, # 26 p. 5612 - 5615
反应条件
air in acetonitrile 0.166667 h; Ambient temperatureIrradiationother reaction time; also under N2 and for thermolysis at 80 deg C; Product distribution;
参考文献
Ogata, Yoshiro; Sawaki, Yasuhiko; Ohno, Takashi
Journal of the American Chemical Society, 1982 , vol. 104, # 1 p. 216 - 219
反应条件
potassium carbonate T=200°C; 6.2 h; Title compound not separated from byproducts;
参考文献
Selva, Maurizio; Marques, Carlos Alberto; Tundo, Pietro
Gazzetta Chimica Italiana, 1993 , vol. 123, # 9 p. 515 - 518
反应条件
1: 69 percent / pyridine / 120 h / Ambient temperature 2: 83 percent / KOH / 2 h / Ambient temperature View Scheme
参考文献
Althoff, Wolfgang; Tinapp, Peter
Archiv der Pharmazie (Weinheim, Germany), 1982 , vol. 315, # 4 p. 289 - 294
参考文献
Ogura,K. et al.
Synthesis, 1979 , p. 880 - 882
参考文献
Ogura,K. et al.
Synthesis, 1979 , p. 880 - 882
