(S)-(-)-叔丁烷硫代亚磺酸叔丁酯合成路线 （共 34 条）
反应条件
3,3-dimethyldioxirane in acetone T=-78°C; 6 h;
参考文献
Journal of Organic Chemistry, , vol. 60, # 4 p. 1044 - 1052
反应条件
3-chloro-benzenecarboperoxoic acid in dichloromethane 1.) 22 - 24 deg C, 3 h, 2.) reflux, 2 h;
参考文献
Journal of Organic Chemistry, , vol. 53, # 6 p. 1263 - 1266
反应条件
3-chloro-benzenecarboperoxoic acid in chloroform-d1 -40 deg C -> 25 deg C;
参考文献
Journal of the American Chemical Society, , vol. 105, # 12 p. 4039 - 4049
反应条件
3-chloro-benzenecarboperoxoic acid in dichloromethane T=22 - 24°C; 10 h; Further byproducts given;
参考文献
Journal of Organic Chemistry, , vol. 53, # 6 p. 1263 - 1266
反应条件
dihydrogen peroxide; acetic acid Ambient temperature;
参考文献
Journal of the American Chemical Society, , vol. 102, p. 4448
反应条件
3-chloro-benzenecarboperoxoic acid in chloroform-d1 T=-55°C; 96 h; other reagent, various time, temp., solvents; Product distributionMechanism;
参考文献
Journal of Organic Chemistry, , vol. 60, # 4 p. 1044 - 1052
反应条件
3-chloro-benzenecarboperoxoic acid in dichloromethane T=22 - 24°C; 10 h; Further byproducts given;
参考文献
Freeman, Fillmore; Lee, Choonsun
Journal of Organic Chemistry, 1988 , vol. 53, # 6 p. 1263 - 1266
反应条件
1: toluene With n-butyllithium; N,N,N',N,-tetramethylethylenediamine in hexane
T=20°C; 0.5 h; Inert atmosphere;
2: di-tert-butyldisulfide S-oxide in tetrahydrofuran; hexane
T=-78°C; 0.5 h; Inert atmosphere;
参考文献
Syed, Majid Khalil; Casey, Mike
European Journal of Organic Chemistry, 2011 , # 35 p. 7207 - 7214
反应条件
1: toluene With 2,2,6,6-tetramethyl-piperidine; n-butyllithium; potassium tert-butylate in tetrahydrofuran; hexane
T=-78°C; 0.583333 h; Inert atmosphere;
2: di-tert-butyldisulfide S-oxide in tetrahydrofuran; hexane
0.683333 h; Inert atmosphere;
参考文献
Syed, Majid Khalil; Casey, Mike
European Journal of Organic Chemistry, 2011 , # 35 p. 7207 - 7214
参考文献
Reisenauer, Hans Peter; Mloston, Grzegorz; Romanski, Jaroslaw; Schreiner, Peter R.
European Journal of Organic Chemistry, 2012 , # 18 p. 3408 - 3415
