甲基4-(苄氧基)丁酸酯合成路线 (共 13 条)
反应条件
sulfuric acid T=20°C; 3 h;
参考文献
Udagawa, Shuji; Sakami, Satoshi; Takemura, Takahiro; Sato, Mikiya; Arai, Takahiro; Nitta, Aiko; Aoki, Takumi; Kawai, Koji; Iwamura, Tomokatsu; Okazaki, Seiji; Takahashi, Takehiro; Kaino, Mie
Bioorganic and Medicinal Chemistry Letters, 2013 , vol. 23, # 6 p. 1617 - 1621
反应条件
Ca(OCl)2 in acetonitrile T=20°C; 0.166667 h;
参考文献
Fisher, Thomas J.; Dussault, Patrick H.
Tetrahedron Letters, 2010 , vol. 51, # 42 p. 5615 - 5617
反应条件
sulfuric acid in methanol
参考文献
Cano, Ivan Collado; Dominianni, Samuel James; Etgen, Garret Jay; Garcia-Paredes, Cristina; Johnston, Richard Duane; Letourneau, Michael Edward; Mantlo, Nathan Bryan; Martinelli, Michael John; Mayhugh, Daniel Ray; Saeed, Ashraf; Thompson, Richard Craig; Wang, Xiaodong; Coffey, David Scott; Schmid, Christopher Randall; Vicenzi, Jeffrey Thomas; Xu, Yanping
Patent: US2004/102500 A1, 2004 ;
反应条件
methanol; PPh3 gold(I) chloro complex; oxygen; AgNTf2 T=25°C;
参考文献
Das, Arindam; Chaudhuri, Rupsha; Liu, Rai-Shung
Chemical Communications, 2009 , # 27 p. 4046 - 4048
反应条件
1: Jones reagent / acetone / 0.5 h 2: 2.56 g / aq. H2SO4 / 3 h / Heating View Scheme
参考文献
Sheehan,M. et al.
Journal of Organic Chemistry, 1971 , vol. 36, p. 3526 - 3532
反应条件
1: 12.0 g / LiAlH4; AlCl3 / CH2Cl2; diethyl ether / 2 h / Heating 2: Jones reagent / acetone / 0.5 h 3: 2.56 g / aq. H2SO4 / 3 h / Heating View Scheme
参考文献
Yamauchi, Noriaki; Endoh, Satoshi; Kato, Keiko; Murae, Tatsushi
Bulletin of the Chemical Society of Japan, 2001 , vol. 74, # 11 p. 2199 - 2205
反应条件
1: p-TsOH / benzene / 12 h / Heating 2: 12.0 g / LiAlH4; AlCl3 / CH2Cl2; diethyl ether / 2 h / Heating 3: Jones reagent / acetone / 0.5 h 4: 2.56 g / aq. H2SO4 / 3 h / Heating View Scheme
参考文献
Yamauchi, Noriaki; Endoh, Satoshi; Kato, Keiko; Murae, Tatsushi
Bulletin of the Chemical Society of Japan, 2001 , vol. 74, # 11 p. 2199 - 2205
反应条件
1: (i) NaH, benzene, (ii) /BRN= 385801/ 2: CrO3, H2SO4 View Scheme
参考文献
Sheehan,M. et al.
Journal of Organic Chemistry, 1971 , vol. 36, p. 3526 - 3532
反应条件
potassium hydroxide 1.)toluene, reflux; Multistep reaction;
参考文献
Hoye, Thomas R.; Kurth, Mark J.; Lo, Vincent
Tetrahedron Letters, 1981 , vol. 22, p. 815 - 818
参考文献
Iwamura,H. et al.
Bulletin of the Chemical Society of Japan, 1976 , vol. 49, p. 1690 - 1696
Full Text Show Details
Sheehan,M. et al.
Journal of Organic Chemistry, 1971 , vol. 36, p. 3526 - 3532