1-(4-甲氧苯基)-2-硝基乙烯合成路线 （共 57 条）
反应条件
tert.-butylhydroperoxide; n-butyllithium in tetrahydrofuran; hexane; toluene
T=-20°C; 1.5 h;
参考文献
Ashwell, Mark A.; Jackson, Richard F. W.
Synthesis, 1988 , # 3 p. 229 - 231
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene
T=20°C; 1 h;
参考文献
Tripathi, Rama P.; Bisht, Surendra Singh; Pandey, Vivek Parashar; Pandey, Sarvesh K.; Singh, Shubhra; Sinha, Sudhir Kumar; Chaturvedi, Vinita
Medicinal Chemistry Research, 2011 , vol. 20, # 9 p. 1515 - 1522
反应条件
1,4-diaza-bicyclo[2.2.2]octane
T=40°C; 1.5 h;
参考文献
Yan, Ming-Chung; Jang, Yeong-Jiunn; Kuo, Wen-Yu; Tu, Zhijay; Shen, Kao-Hsien; Cuo, Ting-Shen; Ueng, Chuen-Her; Yao, Ching-Fa
Heterocycles, 2002 , vol. 57, # 6 p. 1033 - 1048
反应条件
aluminum oxide; triethylamine
1.) CH2Cl2, RT; Yield given. Multistep reaction;
参考文献
Ono, Noboru; Sugi, Kiyoshi; Ogawa, Takuji; Aramaki, Shinji
Journal of the Chemical Society, Chemical Communications, 1993 , # 23 p. 1781 - 1782
反应条件
1: LiAlH4
2: ethanol / Behandeln des Reaktionsprodukts mit wss.-methanol.NH3
View Scheme
参考文献
Bernstein et al.
Journal of the American Chemical Society, 1951 , vol. 73, p. 906,908
反应条件
1: pyridine; bromine / cyclohexane / Inert atmosphere; Reflux
2: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / tetrahydrofuran; water / 20 °C / Inert atmosphere; Reflux
View Scheme
参考文献
Greger, Jessica G.; Yoon-Miller, Sarah J. P.; Bechtold, Nathan R.; Flewelling, Scott A.; MacDonald, Jacob P.; Downey, Catherine R.; Cohen, Eric A.; Pelkey, Erin T.
Journal of Organic Chemistry, 2011 , vol. 76, # 20 p. 8203 - 8214
反应条件
triethylamine; calcium chloride
T=20°C; Michael Addition; 0.5 h; Milling;
参考文献
Jia, Chunman; Chen, Da; Zhang, Chunyan; Zhang, Qi; Cao, Bennan; Zhao, Zhendong
Tetrahedron, 2013 , vol. 69, # 35 p. 7320 - 7324
