N-苄基-N-(1-苯基乙基)胺合成路线 （共 52 条）
反应条件
3 platinum on carbon; hydrogen in toluene T=105°C; P=4500.45 Torr; Flow reactor;
参考文献
Sharma, Sumeet K.; Lynch, James; Sobolewska, Anna M.; Plucinski, Pawel; Watson, Robert J.; Williams, Jonathan M. J.
Catalysis Science and Technology, 2013 , vol. 3, # 1 p. 85 - 88
反应条件
1: benzene / Heating 2: SmBr2 / tetrahydrofuran / 12 h View Scheme
参考文献
Brune, Hans-Albert; Unsin, Josef; Hemmer, Reinhard; Reichhardt, Monika
Journal of Organometallic Chemistry, 1989 , vol. 369, p. 335 - 342
反应条件
caesium carbonate in N,N-dimethyl-formamide T=23°C; 5 h;
参考文献
Salvatore, Ralph Nicholas; Nagle, Advait S.; Kyung, Woon Jung
Journal of Organic Chemistry, 2002 , vol. 67, # 3 p. 674 - 683
反应条件
1: With Cp*Ti(NXylN)(Nt-Bu)(NH2t-Bu) in toluene T=105°C; 24 h; 2: With sodium cyanoborohydride; zinc(II) chloride in methanol; toluene T=20°C; 20 h; regioselective reaction;
参考文献
Weitershaus, Katharina; Ward, Benjamin D.; Kubiak, Raphael; Mueller, Carsten; Wadepohl, Hubert; Doye, Sven; Gade, Lutz H.
Dalton Transactions, 2009 , # 23 p. 4586 - 4602
反应条件
1: ethanol / 3 h / Heating 2: NaBH4 / 72 h / 20 °C View Scheme
参考文献
Brune, Hans-Albert; Unsin, Josef; Hemmer, Reinhard; Reichhardt, Monika
Journal of Organometallic Chemistry, 1989 , vol. 369, p. 335 - 342
反应条件
1,1,3,3-tetramethyldisiloxane; C25H23N3O2; copper(II) bis(trifluoromethanesulfonate) in toluene T=100°C; 24 h; Inert atmosphere;
参考文献
Das, Shoubhik; Join, Benoit; Junge, Kathrin; Beller, Matthias
Chemical Communications, 2012 , vol. 48, # 21 p. 2683 - 2685
反应条件
copper acetylacetonate; water; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'- binaphthyl in o-di-fluorobenzene T=120°C; 2 h; Sealed tube; Reagent/catalyst;
参考文献
Aziz, Jessy; Brion, Jean-Daniel; Hamze, Abdallah; Alami, Mouad
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 11-12 p. 2417 - 2429
反应条件
1: benzene / Heating 2: SmBr2 / tetrahydrofuran / 12 h View Scheme
参考文献
Enders, Dieter; Rembiak, Andreas; Seppelt, Matthias
Tetrahedron Letters, 2013 , vol. 54, # 6 p. 470 - 473
反应条件
tri-n-butyl-tin hydride in N,N-dimethyl-formamide T=20°C; Reductive amination; 7 h;
参考文献
Suwa, Toshihiro; Sugiyama, Erika; Shibata, Ikuya; Baba, Akio
Synlett, 2000 , # 4 p. 556 - 558
反应条件
sodium hydroxide; zinc in water 7.2 h; Ambient temperature;
参考文献
Tsukinoki, Takehito; Mitoma, Yoshiharu; Nagashima, Satoko; Kawaji, Takatoshi; Hashimoto, Iwao; Tashiro, Masashi
Tetrahedron Letters, 1998 , vol. 39, # 48 p. 8873 - 8876
