N-苄基-N-(1-苯基乙基)胺合成路线 （共 52 条）
反应条件
1: 98.7 percent / NaHCO3; 4 Angstroem molecular sieves / benzene / Heating 2: 94 percent / aq. 2-propanol / [Ru2(CO)4(μ-H)(C4Ph4COHOCC4Ph4)] / benzene / 4 h / 70 °C View Scheme
参考文献
Brune, Hans-Albert; Unsin, Josef; Hemmer, Reinhard; Reichhardt, Monika
Journal of Organometallic Chemistry, 1989 , vol. 369, p. 335 - 342
反应条件
palladium diacetate; triphenylphosphine in tetrahydrofuran T=110°C; P=15514.9 Torr; 10 h;
参考文献
Troisi, Luigino; Granito, Catia; Rosato, Francesca; Videtta, Valeria
Tetrahedron Letters, 2010 , vol. 51, # 2 p. 371 - 373
反应条件
palladium diacetate; triphenylphosphine in tetrahydrofuran T=110°C; P=15514.9 Torr; 20 h;
参考文献
Troisi, Luigino; Granito, Catia; Rosato, Francesca; Videtta, Valeria
Tetrahedron Letters, 2010 , vol. 51, # 2 p. 371 - 373
反应条件
[Ir(η5-C5Me5)(C6H4-2-C3H5N2)(NCCH3)](PF6) in N-dodecane; toluene T=100°C; 0.25 h; Inert atmosphere;
参考文献
Blacker, A. John; Stirling, Matthew J.; Page, Michael I.
Organic Process Research and Development, 2007 , vol. 11, # 3 p. 642 - 648
反应条件
1: 85 percent / K2CO3 / dimethylformamide 2: 91 percent / Ni(dppp)Cl2; t-BuMgCl / hexane; diethyl ether / 6 h / 25 °C View Scheme
参考文献
Wehn, Paul M.; Du Bois
Organic Letters, 2005 , vol. 7, # 21 p. 4685 - 4688
反应条件
1: 78 percent / Rh2(OAc)4; PhI(OAc)2; MgO / CH2Cl2 2: 85 percent / K2CO3 / dimethylformamide 3: 91 percent / Ni(dppp)Cl2; t-BuMgCl / hexane; diethyl ether / 6 h / 25 °C View Scheme
参考文献
Wehn, Paul M.; Du Bois
Organic Letters, 2005 , vol. 7, # 21 p. 4685 - 4688
反应条件
sulfuric acid in ethanol
参考文献
Gajda,T. et al.
Synthesis, 1979 , p. 549 - 552
反应条件
in dichloromethane T=20°C;
参考文献
Peterson, Matt A.; Bowman, Adam; Morgan, Sarah
Synthetic Communications, 2002 , vol. 32, # 3 p. 443 - 448
反应条件
1: (i) AcOH, H2SO4, (ii) /BRN= 1905149/ 2: (i) <nBu4N>HSO4, NaOH, K2CO3, benzene, (ii) /BRN= 471308/ 3: aq. H2SO4 / ethanol View Scheme
参考文献
Gajda,T. et al.
Synthesis, 1979 , p. 549 - 552
反应条件
1: (i) <nBu4N>HSO4, NaOH, K2CO3, benzene, (ii) /BRN= 471308/ 2: aq. H2SO4 / ethanol View Scheme
参考文献
Gajda,T. et al.
Synthesis, 1979 , p. 549 - 552
