N-苄基-N-(1-苯基乙基)胺合成路线 （共 52 条）
反应条件
1.1: / toluene / 7 h / 130 °C / 37503.8 Torr / Continuous flow recycle reactor 2.1: methanol / 2 h / 20 °C 2.2: 16 h / 20 - 28 °C View Scheme
参考文献
Cui, Xinjiang; Dai, Xingchao; Deng, Youquan; Shi, Feng
Chemistry - A European Journal, 2013 , vol. 19, # 11 p. 3665 - 3675
反应条件
(S)-4-(pentafluorophenyl)-4,5-dihydro-3H-dinaphtho[2,1-c:1',2'-e]borepine tetrahydrofuran in tetrahydrofuran T=20°C; Reagent/catalyst;
参考文献
Hermeke, Julia; Mewald, Marius; Oestreich, Martin
Journal of the American Chemical Society, 2013 , vol. 135, # 46 p. 17537 - 17546
反应条件
samarium diiodide; water; triethylamine in tetrahydrofuran 0.5 h; Title compound not separated from byproducts;
参考文献
Kim, Myeongseob; Knettle, Brian W.; Dahlen, Anders; Hilmersson, Goeran; Flowers II, Robert A.
Tetrahedron, 2003 , vol. 59, # 52 p. 10397 - 10402
反应条件
tri-ruthenium(0)dodecacarbonyl T=130°C; 24 h; Inert atmosphere;
参考文献
Tillack, Annegret; Hollmann, Dirk; Mevius, Kathleen; Michalik, Dirk; Baehn, Sebastian; Beller, Matthias
European Journal of Organic Chemistry, 2008 , # 28 p. 4745 - 4750
反应条件
1: tris(pentafluorophenyl)-borane; 1,4-diaza-bicyclo[2.2.2]octane / 4 h / 100 °C / |Inert atmosphere 2: water / dichloromethane 3: toluene-4-sulfonic acid / toluene; water / |Inert atmosphere; |Reflux 4: 1-(4,4,5,5-tetramethyl-1,3,2-dioxaboronia-2-yl)-1,4-diazabicyclo[2.2.2]octane tetrakis-(pentafluorophenyl)borate / 4 h / 20 °C / |Inert atmosphere 5: water / dichloromethane View Scheme
参考文献
Eisenberger, Patrick; Bailey, Adrian M.; Crudden, Cathleen M.
Journal of the American Chemical Society, 2012 , vol. 134, # 42 p. 17384 - 17387
反应条件
in N,N-dimethyl-formamide electrolysis of solution containing TBAI;
参考文献
Hess; Marleneziebig
Pharmazie, 1982 , vol. 37, # 2 p. 107 - 111
反应条件
1: triethylamine / dichloromethane / 20 °C / Inert atmosphere 2: C25H23N3O2; 1,1,3,3-tetramethyldisiloxane; copper(II) bis(trifluoromethanesulfonate) / toluene / 24 h / 100 °C / Inert atmosphere View Scheme
参考文献
Das, Shoubhik; Join, Benoit; Junge, Kathrin; Beller, Matthias
Chemical Communications, 2012 , vol. 48, # 21 p. 2683 - 2685
反应条件
1: toluene / |Molecular sieve; |Inert atmosphere 2: (S)-4-(pentafluorophenyl)-4,5-dihydro-3H-dinaphtho[2,1-c:1',2'-e]borepine tetrahydrofuran / tetrahydrofuran / 20 °C View Scheme
参考文献
Hermeke, Julia; Mewald, Marius; Oestreich, Martin
Journal of the American Chemical Society, 2013 , vol. 135, # 46 p. 17537 - 17546
反应条件
1: toluene / |Molecular sieve; |Inert atmosphere 2: (S)-4-(pentafluorophenyl)-4,5-dihydro-3H-dinaphtho[2,1-c:1',2'-e]borepine tetrahydrofuran / tetrahydrofuran / 20 °C View Scheme
参考文献
Hermeke, Julia; Mewald, Marius; Oestreich, Martin
Journal of the American Chemical Society, 2013 , vol. 135, # 46 p. 17537 - 17546
反应条件
in diethyl ether T=20°C; 0.5 h; other solvent (THF), other temperature (-40 deg C), various ratios of reactants; Product distribution;
参考文献
Gracheva, R. A.; Potapov, V. M.; Sivov, N. A.; Sivova, L. I.
Journal of Organic Chemistry USSR (English Translation), 1981 , vol. 17, p. 1963 - 1970
Zhurnal Organicheskoi Khimii, 1981 , vol. 17, # 10 p. 2201 - 2209
