9-胺-1,2,3,4-四氢盐酸氯酯合成路线 （共 22 条）
反应条件
1.1: benzyltrimethylammonium tribromide / acetic acid / 70 °C 1.2: 39 percent / ZnCl2 / 3 h / 70 °C 2.1: 27 percent / aq. sodium hydroxide; nickel-aluminum alloy / dioxane / 3 h / Irradiation View Scheme
参考文献
Heterocycles, , vol. 57, # 9 p. 1683 - 1688
反应条件
p-cresol; ammonia T=180°C;
参考文献
Journal of the Society of Chemical Industry, London, , vol. 64, p. 169,170
反应条件
methanol; bromine; sodium methylate Erwaermen des Reaktionsprodukts mit wss. H2SO4;
参考文献
Collection of Czechoslovak Chemical Communications, , vol. 23, p. 1319
反应条件
zinc(II) chloride Friedlaender synthesis; 2.5 h; Reflux;
参考文献
Journal of Heterocyclic Chemistry, , vol. 49, # 3 p. 533 - 542
反应条件
1: phosphoryl chloride 2: p-cresol; NH3 / 180 °C View Scheme
参考文献
Journal of the Society of Chemical Industry, London, , vol. 64, p. 169,170
反应条件
Yield given. Multistep reaction;
参考文献
Synthesis, , # 5 p. 547 - 548
反应条件
copper dichloride; isopentyl nitrite in acetonitrile T=65°C; Sandmeyer reaction; 2 h; Inert atmosphere;
参考文献
Da Silva, Daniel; Samadi, Abdelouahid; Chioua, Mourad; Do Carmo Carreiras, Maria; Marco-Contelles, Jose
Synthesis, 2010 , # 16 art. no. P05210SS, p. 2725 - 2730
反应条件
triethylamine T=110°C; Cooling with ice;
参考文献
Shen, Yanhong; Yu, Youzhu; Lv, Huichao; Feng, Liping; Zhang, Guoqiang
Letters in Drug Design and Discovery, 2010 , vol. 7, # 5 p. 341 - 345
反应条件
sodium hydride 1) DMF, 90 deg C, 3h 2) DMF, 90 deg C, 3h; Multistep reaction;
参考文献
Asthana, Pratibha; Prasad, Mohan; Rastogi, Shri Nivas
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1987 , vol. 26, p. 330 - 334
参考文献
Petrow
Journal of the Chemical Society, 1947 , p. 634,637
