2-(二甲基乙烯基硅)吡啶合成路线 （共 11 条）
反应条件
1: 2-bromo-pyridine With n-butyllithium in diethyl ether; hexane T=-78°C; 1.5 h; 2: vinyl-dimethyl-chlorosilane in diethyl ether; hexane T=-78 - 20°C; Further stages.;
参考文献
Itami; Mitsudo; Kamei; Koike; Nokami; Yoshida
Journal of the American Chemical Society, 2000 , vol. 122, # 48 p. 12013 - 12014
反应条件
tri-ruthenium(0)dodecacarbonyl in toluene T=100°C; Pauson-Khand reaction; P=760 Torr; Title compound not separated from byproducts;
参考文献
Itami, Kenichiro; Mitsudo, Koichi; Fujita, Kazuyoshi; Ohashi, Youichi; Yoshida, Jun-Ichi
Journal of the American Chemical Society, 2004 , vol. 126, # 35 p. 11058 - 11066
反应条件
tetrabutyl ammonium fluoride; bis(benzonitrile)palladium(II) dichloride in tetrahydrofuran
T=60°C;
参考文献
Itami; Nokami; Yoshida
Journal of the American Chemical Society, 2001 , vol. 123, # 23 p. 5600 - 5601
反应条件
1: carbon monoxide; dimethyl(2-pyridinyl)(vinyl)silane With tri-ruthenium(0)dodecacarbonyl in toluene
T=100°C; Pauson-Khand-type reaction; P=760 Torr; 0.166667 h;
2: benzene, 1-methyl-4-(1-propynyl)- in toluene
T=100°C; 24 h;
参考文献
Itami, Kenichiro; Mitsudo, Koichi; Fujita, Kazuyoshi; Ohashi, Youichi; Yoshida, Jun-Ichi
Journal of the American Chemical Society, 2004 , vol. 126, # 35 p. 11058 - 11066
反应条件
1: carbon monoxide; dimethyl(2-pyridinyl)(vinyl)silane With tri-ruthenium(0)dodecacarbonyl in toluene
T=100°C; Pauson-Khand-type reaction; P=760 Torr; 0.166667 h;
2: 1-chloro-4-(1-propynyl)-benzene in toluene
T=100°C; 24 h;
参考文献
Itami, Kenichiro; Mitsudo, Koichi; Fujita, Kazuyoshi; Ohashi, Youichi; Yoshida, Jun-Ichi
Journal of the American Chemical Society, 2004 , vol. 126, # 35 p. 11058 - 11066
反应条件
tri-ruthenium(0)dodecacarbonyl in xylene
T=120°C; Pauson-Khand reaction; P=760 Torr;
参考文献
Itami, Kenichiro; Mitsudo, Koichi; Fujita, Kazuyoshi; Ohashi, Youichi; Yoshida, Jun-Ichi
Journal of the American Chemical Society, 2004 , vol. 126, # 35 p. 11058 - 11066
反应条件
tri-ruthenium(0)dodecacarbonyl in toluene
T=100°C; Pauson-Khand reaction; P=760 Torr;
参考文献
Itami, Kenichiro; Mitsudo, Koichi; Fujita, Kazuyoshi; Ohashi, Youichi; Yoshida, Jun-Ichi
Journal of the American Chemical Society, 2004 , vol. 126, # 35 p. 11058 - 11066
反应条件
1: carbon monoxide; dimethyl(2-pyridinyl)(vinyl)silane With tri-ruthenium(0)dodecacarbonyl in toluene
T=100°C; Pauson-Khand-type reaction; P=760 Torr; 0.166667 h;
2: 1-(p-CH3O)phenylprop-1-yne in toluene
T=100°C; 24 h;
参考文献
Itami, Kenichiro; Mitsudo, Koichi; Fujita, Kazuyoshi; Ohashi, Youichi; Yoshida, Jun-Ichi
Journal of the American Chemical Society, 2004 , vol. 126, # 35 p. 11058 - 11066
反应条件
tri-ruthenium(0)dodecacarbonyl in toluene
T=100°C; Pauson-Khand reaction; P=760 Torr;
参考文献
Itami, Kenichiro; Mitsudo, Koichi; Yoshida, Jun-Ichi
Angewandte Chemie - International Edition, 2002 , vol. 41, # 18 p. 3481 - 3484
反应条件
tri-ruthenium(0)dodecacarbonyl in toluene
T=100°C; Pauson-Khand reaction; P=760 Torr;
参考文献
Itami, Kenichiro; Mitsudo, Koichi; Fujita, Kazuyoshi; Ohashi, Youichi; Yoshida, Jun-Ichi
Journal of the American Chemical Society, 2004 , vol. 126, # 35 p. 11058 - 11066
