3-溴-1-甲基-碘化吡啶合成路线 (共 5 条)
反应条件
ethanol T=92°C; 16 h; Inert atmosphereReflux;
参考文献
Ormond-Prout, Johnathan E.; Smart, Paul; Brammer, Lee
Crystal Growth and Design, 2012 , vol. 12, # 1 p. 205 - 216
反应条件
1-methyl-1H-imidazole T=200°C; 0.25 h;
参考文献
Deady, Leslie W.; Finlayson, Wayne L.
Synthetic Communications, 1980 , vol. 10, # 12 p. 947 - 950
反应条件
in acetonitrile T=25°C; ΔG(excit.), ΔH(excit.), ΔS(excit.); KineticsEquilibrium constantThermodynamic data;
参考文献
Arnett, Edward M.; Reich, Ronald
Journal of the American Chemical Society, 1980 , vol. 102, # 18 p. 5892 - 5902
反应条件
sodium tetrahydroborate in methanol
T=-15°C; 0.5 h;
参考文献
Drinkuth, Stefan; Groetsch, Stefan; Peters, Eva-Maria; Peters, Karl; Christl, Manfred
European Journal of Organic Chemistry, 2001 , # 14 p. 2665 - 2670
反应条件
tris-(o-tolyl)phosphine; tris(dibenzylideneacetone)dipalladium (0) in N,N-dimethyl-formamide
T=20°C; Stille reaction;
参考文献
Garcia-Cuadrado, Domingo; Cuadro, Ana M.; Alvarez-Builla, Julio; Vaquero, Juan Jose
Synlett, 2002 , # 11 p. 1904 - 1906