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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
32228-16-3
合成路线
（共 9 条）
536-74-3
苯乙炔
+
106-54-7
4-氯苯硫酚
→
反应条件
32228-21-0
反应条件
diphosphino-functionalized MCM-41 anchored rhodium complex [MCM-41-2P-RhCl(PPh3)] in ethanol T=40°C; 24 h; Inert atmosphere; stereoselective reaction;
参考文献
Zhao, Hong; Peng, Jian; Cai, Mingzhong
Catalysis Letters, 2012 , vol. 142, # 1 p. 138 - 142
42599-24-6
+
106-54-7
4-氯苯硫酚
→
反应条件
32228-21-0
反应条件
copper(II) oxide; potassium hydroxide in dimethyl sulfoxide T=20 - 80°C; stereoselective reaction;
参考文献
Reddy, Vutukuri Prakash; Swapna, Kokkirala; Kumar, Akkilagunta Vijay; Rao, Kakulapati Rama
Synlett, 2009 , # 17 p. 2783 - 2788
1142-19-4
4,4'-二氯二苯二硫醚
+
588-72-7
→
反应条件
32228-16-3
+
32228-21-0
反应条件
copper(l) iodide; zinc in glycerol T=110°C; 24 h; Inert atmosphere; Overall yield = 60 percent; Overall yield = 0.088 g;
参考文献
Goncalves, Loren C.C.; Lima, David B.; Borba, Pedro M.Y.; Perin, Gelson; Alves, Diego; Jacob, Raquel G.; Lenardao, Eder J.
Tetrahedron Letters, 2013 , vol. 54, # 26 p. 3475 - 3480
536-74-3
苯乙炔
+
933-01-7
→
反应条件
32228-21-0
反应条件
1: phenylacetylene With Schwartz's reagent in tetrahydrofuran T=20°C; Metallation; 0.333333 h; 2: (4-chlorophenyl)sulfenyl chloride in tetrahydrofuran T=20°C; Substitution; 0.5 h;
参考文献
Huang, Xian; Zhong, Ping; Guo, Wei-Rong
Organic Preparations and Procedures International, 1999 , vol. 31, # 2 p. 201 - 203
536-74-3
苯乙炔
+
106-54-7
4-氯苯硫酚
→
反应条件
1373927-38-8
+
32228-16-3
+
32228-21-0
反应条件
[bmim][SeO2(OCH3)] T=60°C; 2 h; Inert atmosphere;
参考文献
Thurow, Samuel; Ostosi, Naiana T.; Mendes, Samuel R.; Jacob, Raquel G.; Lenardao, Eder J.
Tetrahedron Letters, 2012 , vol. 53, # 21 p. 2651 - 2653
106-54-7
4-氯苯硫酚
+
637-44-5
苯丙炔酸
→
反应条件
32228-16-3
+
32228-21-0
反应条件
copper(l) iodide; caesium carbonate in 1-methyl-pyrrolidin-2-one T=90°C; 24 h; optical yield given as percent destereoselective reaction;
参考文献
Ranjit, Sadananda; Duan, Zhongyu; Zhang, Pengfei; Liu, Xiaogang
Organic Letters, 2010 , vol. 12, # 18 p. 4134 - 4136
536-74-3
苯乙炔
+
106-54-7
4-氯苯硫酚
→
反应条件
32228-16-3
+
32228-21-0
反应条件
water T=30°C; 2.7 h; optical yield given as percent deregioselective reaction;
参考文献
Liao, Yunfeng; Chen, Shanping; Jiang, Pengcheng; Qi, Hongrui; Deng, Guo-Jun
European Journal of Organic Chemistry, 2013 , # 30 p. 6878 - 6885
873-73-4
对氯苯乙炔
+
536-74-3
苯乙炔
→
反应条件
32228-16-3
+
32228-21-0
反应条件
[C5mim][BF4] in ethanol T=20°C; 2 h; optical yield given as percent destereoselective reaction;
参考文献
Ranu, Brindaban C.; Chattopadhyay, Kalicharan; Ghosh, Sudip; Jana, Ranjan
Journal of the Indian Chemical Society, 2008 , vol. 85, # 12 p. 1199 - 1204
588-72-7
+
18803-44-6
→
反应条件
32228-21-0
反应条件
copper T=145 - 170°C;
参考文献
Baliah,V.; Rathinasamy,T.K.
Indian Journal of Chemistry, 1971 , vol. 9, p. 220 - 225
