反应条件
1.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -95 °C / Inert atmosphere 1.2: 3 h / -95 °C / Inert atmosphere 2.1: n-butyllithium / tetrahydrofuran; hexane / 0.3 h / -90 °C / Inert atmosphere 2.2: 0.5 h / -90 °C / Inert atmosphere 2.3: -90 °C 3.1: sulfuric acid / tetrahydrofuran; hexane / 0.1 h / -90 °C / Inert atmosphere View Scheme
参考文献
Honda, Mitsunori; Nakae, Kenta; Nishizawa, Toshiaki; Suda, Mitsuhiro; Kunimoto, Ko-Ki; Segi, Masahito
Tetrahedron, 2011 , vol. 67, # 49 p. 9500 - 9508