2-偶氮基环己烯-1-醇合成路线 （共 29 条）
反应条件
1: With 2,5-dioxopyrrolidin-1-yl 3-(diphenylphosphanyl)propanoate in tetrahydrofuran; water 3 h; Inert atmosphere; 2: With sodium hydrogencarbonate in tetrahydrofuran; water 0.25 h; chemoselective reaction;
参考文献
Raines, Ronald Thaddeus; Myers, Eddie Leonard
Patent: US2010/125132 A1, 2010 ;
Location in patent: Page/Page column 32 ;
反应条件
4-toluenesulfonyl azide; potassium carbonate 0.0833333 h;
参考文献
Rao, Y. Koteswar; Nagarajan, M.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1986 , vol. 25, p. 735 - 737
反应条件
4-toluenesulfonyl azide
参考文献
Thoraval, J. Y.; Nagai, W.; Yeung Lam Ko, Y. Y. C.; Carrie, R.
Tetrahedron, 1990 , vol. 46, # 11 p. 3859 - 3868
反应条件
(i) NaH, HCO2Et, Et2O, (ii) 4-azidosulfonyl-benzoic acid, THF; Multistep reaction;
参考文献
McKervey, M. Anthony; Ratananukul, Piniti
Tetrahedron Letters, 1983 , vol. 24, # 1 p. 117 - 120
反应条件
in benzene Irradiationaddition of methanol in the dark after irradiation, nondegassed solvent; Product distributionMechanism;
参考文献
Journal of Organic Chemistry, , vol. 45, # 26 p. 5278 - 5283
反应条件
Irradiationbenzophenone as sensitizer, var. additives, var. solvents; Product distributionMechanism;
参考文献
Journal of Organic Chemistry, , vol. 45, # 26 p. 5278 - 5283
反应条件
in benzene Irradiationaddition of methanol in the dark after irradiation, nondegassed solvent; Product distributionMechanism;
参考文献
Tomioka, Hideo; Okuno, Hiroshi; Izawa, Yasuji
Journal of Organic Chemistry, 1980 , vol. 45, # 26 p. 5278 - 5283
反应条件
Irradiationbenzophenone as sensitizer, var. additives, var. solvents; Product distributionMechanism;
参考文献
Tomioka, Hideo; Okuno, Hiroshi; Izawa, Yasuji
Journal of Organic Chemistry, 1980 , vol. 45, # 26 p. 5278 - 5283
反应条件
in benzene Irradiationaddition of methanol in the dark after irradiation, nondegassed solvent; Product distributionMechanism;
参考文献
Journal of Organic Chemistry, , vol. 45, # 26 p. 5278 - 5283
反应条件
Irradiationbenzophenone as sensitizer, var. additives, var. solvents; Product distributionMechanism;
参考文献
Journal of Organic Chemistry, , vol. 45, # 26 p. 5278 - 5283
