(Z)-十二碳-3-烯-1-醇合成路线 （共 5 条）
反应条件
pyridinium chlorochromate in dichloromethane
2 h;
参考文献
Bestmann; Koschatzky; Schaetzke; et al.
1981 , vol. No. 9, p. 1705 - 1720
反应条件
4-(N,N-dimethlyamino)pyridine; triethylamine in dichloromethane
T=-4°C; 7 h;
参考文献
Hanko, Rudolf; Hammond, Michael D.; Fruchtmann, Romanis; Pfitzner, Joerg; Place, Graham A.
Journal of Medicinal Chemistry, 1990 , vol. 33, # 4 p. 1163 - 1170
反应条件
in acetic acid
T=25 - 35°C; 48 h;
参考文献
Pop, Lidia; Oprean, I.; Barabas, A.; Hodosan, F.
Journal fuer Praktische Chemie (Leipzig), 1986 , vol. 328, # 5/6 p. 867 - 878
反应条件
Multi-step reaction with 3 steps 1: 1) n-butyllithium / 1) THF, -78 deg C, 2) HMPA, room temperature2: 91 percent / H2, quinoline / Pd/BaSO4 / methanol3: 89 percent / Dowex / methanol / 45 °C
参考文献
Carvalho, Joan F.; Prestwich, Glenn D. Journal of Organic Chemistry, 1984 , vol. 49, # 7 p. 1251 - 1258
反应条件
Multi-step reaction with 5 steps 1: 63 percent / piperidine / xylene / Heating2: 83 percent / LAH / diethyl ether3: Br2 / CCl4 4: NaNH2 / CCl4; aq. NH3 / 4 h / -78 °C5: 100 percent / H2 / P-2 Ni / ethanol
参考文献
Pawar, A. S.; Chattopadhyay, S.; Mamdapur, V. R. Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1993 , vol. 32, # 4 p. 463 - 464
