5-(3-吡啶基)-1H-四唑合成路线 （共 9 条）
反应条件
sodium azide in N,N-dimethyl-formamide 24 h; Reflux;
参考文献
Teimouri, Abbas; Najafi Chermahini, Alireza
Polyhedron, 2011 , vol. 30, # 15 p. 2606 - 2610
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran T=25 - 80°C;
参考文献
Sindkhedkar, Milind Dattatraya; Desai, Vijaya Narayan; Loriya, Rajesh Maganlal; Patel, Mahesh Vithalbhai; Trivedi, Bharat Kalidas; Bora, Rajesh Onkardas; Diwakar, Santosh Devidas; Jadhav, Ganesh Rajaram; Pawar, Shivaji Sampatrao
Patent: US2009/247478 A1, 2009 ;
Location in patent: Page/Page column 45 ;
反应条件
bismuth trifluoromethanesulphonate; sodium azide; methanecarbohydroxamic acid in N,N-dimethyl-formamide T=120°C; 15 h;
参考文献
Sridhar, Madabhushi; Mallu, Kishore Kumar Reddy; Jillella, Raveendra; Godala, Kondalreddy; Beeram, Chinaramanaiah; Chinthala, Narsaiah
Synthesis (Germany), 2013 , vol. 45, # 4 art. no. SS-2012-Z0887-OP, p. 507 - 510
反应条件
in water; N,N-dimethyl-formamide
参考文献
Polyhedron, , vol. 55, p. 24 - 36
反应条件
1: 88 percent / Pd(PPh3)4 / dimethylformamide / 0.03 h / microwave irradiation 2: 75 percent / NaN3; NH4Cl / dimethylformamide / 0.25 h / microwave irradiation View Scheme
参考文献
Journal of Organic Chemistry, , vol. 65, # 23 p. 7984 - 7989
反应条件
T=120°C; 0.25 h; Microwave irradiation;
参考文献
Efimova; Artamonova; Koldobskii
Russian Journal of Organic Chemistry, 2008 , vol. 44, # 9 p. 1345 - 1347
反应条件
potassium carbonate in N,N-dimethyl-formamide T=105°C; 0.7 h; Irradiation;
参考文献
Ishmetova, R. I.; Kitaeva, V. G.; Rusinov, L. G.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1993 , vol. 29, # 8 p. 902 - 905
Khimiya Geterotsiklicheskikh Soedinenii, 1993 , # 8 p. 1060 - 1063
反应条件
T=100°C; 1 h; Microwave irradiation;
参考文献
Efimova; Artamonova; Koldobskii
Russian Journal of Organic Chemistry, 2008 , vol. 44, # 9 p. 1345 - 1347
参考文献
Laessig, Daniel; Lincke, Joerg; Krautscheid, Harald
Tetrahedron Letters, 2010 , vol. 51, # 4 p. 653 - 656
