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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
苯硼酸酐
合成路线
(共 274 条)
3262-89-3
苯硼酸酐
+
33617-65-1
→
反应条件
612-94-2
2-苯基萘
反应条件
potassium phosphate; Ni(PCy3)2Cl2; water in 1,4-dioxane T=110°C; 12 h; Inert atmosphere;
参考文献
Guan, Bing-Tao; Wang, Yang; Li, Bi-Jie; Yu, Da-Gang; Shi, Zhang-Jie
Journal of the American Chemical Society, 2008 , vol. 130, # 44 p. 14468 - 14470
3262-89-3
苯硼酸酐
+
359445-23-1
→
反应条件
612-94-2
2-苯基萘
反应条件
potassium phosphate; Ni(PCy3)2Cl2; water in 1,4-dioxane T=110°C; 12 h; Inert atmosphere;
参考文献
Guan, Bing-Tao; Wang, Yang; Li, Bi-Jie; Yu, Da-Gang; Shi, Zhang-Jie
Journal of the American Chemical Society, 2008 , vol. 130, # 44 p. 14468 - 14470
3262-89-3
苯硼酸酐
+
1523-11-1
乙酸-2-萘酯
→
反应条件
612-94-2
2-苯基萘
+
135-19-3
2-萘酚
反应条件
potassium phosphate; Ni(PCy3)2Cl2; water in 1,4-dioxane T=110°C; 12 h; Inert atmosphere;
参考文献
Guan, Bing-Tao; Wang, Yang; Li, Bi-Jie; Yu, Da-Gang; Shi, Zhang-Jie
Journal of the American Chemical Society, 2008 , vol. 130, # 44 p. 14468 - 14470
3262-89-3
苯硼酸酐
+
135-19-3
2-萘酚
→
反应条件
612-94-2
2-苯基萘
反应条件
1: With sodium hydride in tetrahydrofuran T=20°C; Suzuki-Miyaura coupling; 0.0833333 h; Inert atmosphere; 2: With triethyl borane in tetrahydrofuran; hexane T=20°C; Suzuki-Miyaura coupling; 0.0833333 h; Inert atmosphere; 3: With [Ni0(1,5-cyclooctadiene)2]; tri-cyclo-hexyl-phosphine in tetrahydrofuran; hexane; o-xylene T=110°C; Suzuki-Miyaura coupling; 48 h; Inert atmosphere;
参考文献
Yu, Da-Gang; Shi, Zhang-Jie
Angewandte Chemie - International Edition, 2011 , vol. 50, # 31 p. 7097 - 7100
3262-89-3
苯硼酸酐
+
21436-44-2
3-甲基苯-1-羧酸酐
→
反应条件
643-93-6
+
643-65-2
反应条件
potassium fluoride; tetrakis-(ethylene)-μ,μ'-dichlorodirhodium(I) in 1,3,5-trimethyl-benzene T=160°C; Suzuki coupling; 8 h; Product distribution; Further Variations:CatalystsReagentsSolventsTemperatures;
参考文献
Advanced Synthesis and Catalysis, , vol. 346, # 13-15 p. 1665 - 1668
3262-89-3
苯硼酸酐
+
925-90-6
→
反应条件
97-94-9
+
960-71-4
反应条件
in diethyl ether
参考文献
Ber., , vol. 64, p. 2112 - 2116
B: SVol.1, 4.8.3, page 219 - 224
3262-89-3
苯硼酸酐
+
1208405-05-3
→
反应条件
58-72-0
反应条件
Ni(PCy3)2Cl2; potassium carbonate; tri-cyclo-hexyl-phosphine in 1,4-dioxane; water T=110°C; Suzuki-Miyaura coupling; 16 h; Inert atmosphere;
参考文献
Xu, Li; Li, Bi-Jie; Wu, Zhen-Hua; Lu, Xing-Yu; Guan, Bing-Tao; Wang, Bi-Qin; Zhao, Ke-Qing; Shi, Zhang-Jie
Organic Letters, 2010 , vol. 12, # 4 p. 884 - 887
3262-89-3
苯硼酸酐
+
34544-89-3
→
反应条件
58-72-0
反应条件
potassium phosphate; Ni(PCy3)2Cl2; water in 1,4-dioxane; toluene T=110°C; Suzuki-Miyaura coupling; 20 h; Inert atmosphere;
参考文献
Sun, Chang-Liang; Yang, Wang; Xiao, Zhou; Wu, Zhen-Hua; Li, Bi-Jie; Guan, Bing-Tao; Shi, Zhang-Jie
Chemistry - A European Journal, 2010 , vol. 16, # 20 p. 5844 - 5847
3262-89-3
苯硼酸酐
→
反应条件
58-72-0
反应条件
potassium phosphate; Ni(PCy3)2Cl2; water in 1,4-dioxane; toluene T=110°C; Suzuki-Miyaura coupling; 20 h; Inert atmosphere;
参考文献
Sun, Chang-Liang; Yang, Wang; Xiao, Zhou; Wu, Zhen-Hua; Li, Bi-Jie; Guan, Bing-Tao; Shi, Zhang-Jie
Chemistry - A European Journal, 2010 , vol. 16, # 20 p. 5844 - 5847
3262-89-3
苯硼酸酐
+
201230-82-2
+
501-65-5
→
反应条件
4023-77-2
+
58-72-0
+
1801-42-9
反应条件
methanol; bis(1,5-cyclooctadiene)-rhodium(I) tetrafluoroborate T=120°C; P=760.051 Torr; 16 h; Autoclave;
参考文献
Tetrahedron, , vol. 65, # 45 p. 9125 - 9133
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