diimide in methanol Heatingproduct distribution as a function of reaction time; Product distribution;

Hydrogenation;

in N,N-dimethyl-formamide controlled-potential electrolyse; Title compound not separated from byproducts;

tris(dibenzylideneacetone)dipalladium(0) chloroform complex; 1,1'-bis-(diphenylphosphino)ferrocene; acetic acid in tetrahydrofuran T=80°C; 4 h;

1: With manganese(IV) oxide; 2,2,6,6-tetramethyl-1-piperidinyloxy, free radical; copper(II) bis(trifluoromethanesulfonate); (S,S)-tBuBOX in N,N-dimethyl-formamide T=20°C; 15 h; Inert atmosphere; 2: With 3-chloro-benzenecarboperoxoic acid in dichloromethane T=0°C; 0.166667 h; Inert atmosphere; Overall yield = 14.8 mg;

1: With manganese(IV) oxide; 2,2,6,6-tetramethyl-1-piperidinyloxy, free radical; copper(II) bis(trifluoromethanesulfonate); (S,S)-tBuBOX in N,N-dimethyl-formamide T=20°C; 15 h; Inert atmosphere; 2: With 3-chloro-benzenecarboperoxoic acid in dichloromethane T=0°C; 0.166667 h; Inert atmosphere; Overall yield = 14.8 mg;

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