3-(4-甲氧基-苯基)-5-苯基-1H-吡唑合成路线 （共 18 条）
反应条件
1.1: n-butyllithium / tetrahydrofuran / 0.67 h / -78 °C / |Inert atmosphere 1.2: -78 °C / |Inert atmosphere 2.1: boron trifluoride diethyl etherate / acetonitrile / 0.25 h / 20 °C / |Inert atmosphere 3.1: potassium tert-butylate / acetonitrile / 0.5 h / 20 °C / |Inert atmosphere View Scheme
参考文献
Harigae, Ryo; Moriyama, Katsuhiko; Togo, Hideo
Journal of Organic Chemistry, 2014 , vol. 79, # 5 p. 2049 - 2058
反应条件
1: boron trifluoride diethyl etherate / acetonitrile / 0.25 h / 20 °C / |Inert atmosphere 2: potassium tert-butylate / acetonitrile / 0.5 h / 20 °C / |Inert atmosphere View Scheme
参考文献
Raji Reddy, Chada; Vijaykumar, Jonnalagadda; Gree, Rene
Synthesis (Germany), 2013 , vol. 45, # 6 art. no. SS-2012-Z0977-OP, p. 830 - 836
反应条件
1: 5 wt Cu/Fe / 3 h / 100 °C 2: hydrazine hydrate / N,N-dimethyl-formamide / 2 h / 100 °C View Scheme
参考文献
Kovacs, Szabolcs; Novak, Zoltan
Tetrahedron, 2013 , vol. 69, # 43 p. 8987 - 8993
反应条件
sodium peroxodisulphate 0.833333 h; Sealed tubeMillingGreen chemistry;
参考文献
Zhang, Ze; Tan, Ya-Jun; Wang, Chun-Shan; Wu, Hao-Hao
Heterocycles, 2014 , vol. 89, # 1 p. 103 - 112
反应条件
1: hydrazine hydrate / 0.67 h / 20 °C / |Sealed tube; |Milling; |Green chemistry 2: sodium peroxodisulphate / 0.83 h / |Sealed tube; |Milling; |Green chemistry View Scheme
参考文献
Zhang, Ze; Tan, Ya-Jun; Wang, Chun-Shan; Wu, Hao-Hao
Heterocycles, 2014 , vol. 89, # 1 p. 103 - 112
参考文献
Joerlander
Chemische Berichte, 1916 , vol. 49, p. 2792
参考文献
Joerlander
Chemische Berichte, 1916 , vol. 49, p. 2792
参考文献
Freudenberg; Stoll
Justus Liebigs Annalen der Chemie, 1924 , vol. 440, p. 42
