Abdur-Rashid, Kamaluddin; Fong, Tina P.; Greaves, Bronwyn; Gusev, Dmitry G.; Hinman, Justin G.; Landau, Shaun E.; Lough, Alan J.; Morris, Robert H.
Journal of the American Chemical Society, 2000 , vol. 122, # 38 p. 9155 - 9171
in methanol (N2); dropwise addn. of a soln. of phosphine to a soln. of Pd-complex; stirring for 1 h; filtration; washing with methanol; 3 times recrystn. from MeOH/CH2Cl2 (1:1); elem. anal.;
参考文献
Journal of Physical Chemistry, , vol. 94, # 16 p. 6255 - 6263
Abdur-Rashid, Kamaluddin; Fong, Tina P.; Greaves, Bronwyn; Gusev, Dmitry G.; Hinman, Justin G.; Landau, Shaun E.; Lough, Alan J.; Morris, Robert H.
Journal of the American Chemical Society, 2000 , vol. 122, # 38 p. 9155 - 9171
potassium tert-butylate in tetrahydrofuran
60°C, overnight, under N2; THF evapd. in vac., the residue extd. with toluene, filtered, the soln.evapd. in vac., the residue pumped in vac. at 65°C, the residue dissolved in heptane and filtered, pptn. by cooling to -20°C, thecrystals dried in vac.; elem. anal.;
参考文献
Mann, Brian E.; Musco, Alfredo
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1980 , p. 776 - 785
