四(二甲基氨基)钛(IV)合成路线 （共 11 条）
反应条件
in benzene-d6 byproducts: HNMe2, HSi(SiMe3)3; N2-atmosphere; 1 equiv. water, 4 h; not isolated, detd. by NMR spectroscopy;
参考文献
Inorganic Chemistry, , vol. 37, # 24 p. 6366 - 6372
反应条件
diethyl ether; benzene
参考文献
Proceedings of the Chemical Society, London, , p. 225
Journal of the Chemical Society, , p. 3857,3860
反应条件
in neat (no solvent) N2-atmosphere; distn. (vac.);
参考文献
Journal of Organometallic Chemistry, , vol. 528, # 1-2 p. 195 - 198
反应条件
in toluene N2-atmosphere; equimolar amts., stirring for 3 h; crystn. (-35°C; two crops), collection (filtration), washing (pentane), drying (vac.); elem. anal.;
参考文献
Johnson; Lee; Odom; Davis; Cummins
Angewandte Chemie - International Edition in English, 1997 , vol. 36, # 1-2 p. 87 - 91
参考文献
Chandra,G. et al.
Journal of the Chemical Society [Section] C: Organic, 1969 , p. 2565 - 2568
反应条件
in dichloromethane T=0°C; 0.5 h;
参考文献
Hosomi, Akira; Yanagi, Toshiharu; Hojo, Makoto
Tetrahedron Letters, 1991 , vol. 32, # 21 p. 2371 - 2374
反应条件
in tetrahydrofuran Heating;
参考文献
Wilson,J.D. et al.
Journal of Organic Chemistry, 1971 , vol. 36, p. 1613 - 1615
参考文献
Froneman, M.; Cheney, D. L.; Modro, T. A.
Phosphorus, Sulfur and Silicon and the Related Elements, 1990 , vol. 47, p. 273 - 281
参考文献
Froneman, M.; Cheney, D. L.; Modro, T. A.
Phosphorus, Sulfur and Silicon and the Related Elements, 1990 , vol. 47, p. 273 - 281
反应条件
sulfur dioxide in Petroleum ether
参考文献
Chandra,G. et al.
Journal of the Chemical Society [Section] C: Organic, 1969 , p. 2565 - 2568
