1,1,3,3-四甲基二硅氧烷合成路线 （共 158 条）
反应条件
tetrabutylammomium bromide in water
参考文献
Shin-Etsu Chemical Co., Ltd.
Patent: EP461597 A2, 1991 ;
参考文献
Shin-Etsu Chemical Co., Ltd.
Patent: US4096161 A1, 1978 ;
参考文献
Basenko; Voronkov; Zelenkov; Albanov
Doklady Chemistry, 2011 , vol. 439, # 2 p. 219 - 222
反应条件
hydrogenchloride T=-10°C; other temperatures, also addition of saturated aq. NaCl, 25 percent aq. CaCl2, CaCl2 and LiCl; Product distributionEquilibrium constant;
参考文献
Emeleus; Onyszchuk
Journal of the Chemical Society, 1958 , p. 604,606
反应条件
lithium bromide in N-methyl-acetamide; dichloromethane; acetonitrile
参考文献
SmithKline Beecham Corporation
Patent: US5602173 A1, 1997 ;
US 5602173 A
反应条件
lithium bromide in dichloromethane; acetonitrile
参考文献
SmithKline Beecham Corporation
Patent: US5449686 A1, 1995 ;
反应条件
lithium bromide in N-methyl-acetamide; dichloromethane; acetonitrile
参考文献
SmithKline Beecham Corporation
Patent: US5605923 A1, 1997 ;
US 5605923 A
反应条件
1: Ph2Si(OH)2 With tris(pentafluorophenyl)-borane in anhydrous xylene T=40°C; Inert atmosphere; 2: 1,1,3,3-tetramethyldisiloxane in anhydrous xylene T=40 - 60°C; 2 h; Inert atmosphere; Reagent/catalyst;
参考文献
SIVANCE LLC; Wilson, Michael E.
Patent: US2013/79539 A1, 2013 ;
Location in patent: Paragraph 0017 ;
反应条件
dihydrogen hexachloroplatinate in ethylhexanol, 2- T=70 - 80°C; 2.5 h;
参考文献
Shin-Etsu Chemical Co., Ltd.
Patent: EP1867652 A1, 2007 ;
Location in patent: Page/Page column 9 ;
反应条件
ruthenium trichloride T=40 - 70°C; 7 - 19 h; Product distribution / selectivity;
参考文献
SHIN-ETSU CHEMICAL CO., LTD.
Patent: US2007/37997 A1, 2007 ;
Location in patent: Page/Page column 5 ;
