(4-氯苯基)(环己基)甲酮合成路线 （共 14 条）
反应条件
1: 82 percent / tetrahydrofuran / 1 h / 60 °C 2: 96 percent / p-toluenesulfonic acid / toluene / 1 h / Heating 3: 44 percent / N-bromoacetamide (NBA), H2O / acetone / 6 h / Ambient temperature 4: 51 percent / dimethylformamide / 18 h / 100 °C View Scheme
参考文献
Heterocycles, , vol. 31, # 3 p. 537 - 548
反应条件
1: 82 percent / tetrahydrofuran / 1 h / 60 °C 2: 96 percent / p-toluenesulfonic acid / toluene / 1 h / Heating 3: 44 percent / N-bromoacetamide (NBA), H2O / acetone / 6 h / Ambient temperature 4: 51 percent / dimethylformamide / 18 h / 100 °C View Scheme
参考文献
Heterocycles, , vol. 31, # 3 p. 537 - 548
反应条件
1: sodium hexamethyldisilazane / |Inert atmosphere; |Schlenk technique 2: diisobutylaluminium hydride / |Inert atmosphere; |Schlenk technique 3: iron tribromide / toluene / 14 h / 130 °C / |Sealed tube; |Schlenk technique; |Inert atmosphere View Scheme
参考文献
Journal of the American Chemical Society, , vol. 135, # 34 p. 12576 - 12579
反应条件
1: diisobutylaluminium hydride / |Inert atmosphere; |Schlenk technique 2: iron tribromide / toluene / 14 h / 130 °C / |Sealed tube; |Schlenk technique; |Inert atmosphere View Scheme
参考文献
Journal of the American Chemical Society, , vol. 135, # 34 p. 12576 - 12579
