2-氯-5-甲酰基苯磺酰胺合成路线 （共 5 条）
反应条件
manganese(IV) oxide in acetone 50 h;
参考文献
SMITHKLINE BEECHAM CORPORATION
Patent: WO2005/82890 A1, 2005 ;
Location in patent: Page/Page column 73 ;
WO 2005/082890 A1
反应条件
in formic acid; water
参考文献
Hoechst Aktiengesellschaft
Patent: US4156732 A1, 1979 ;
反应条件
hydrogenchloride in ethanol Heating;
参考文献
Loynes,J.M. et al.
Journal of Medicinal Chemistry, 1965 , vol. 8, p. 691 - 694
反应条件
1: CrO3, H2SO4 / acetic acid 2: aq. HCl / ethanol / Heating View Scheme
参考文献
Loynes,J.M. et al.
Journal of Medicinal Chemistry, 1965 , vol. 8, p. 691 - 694
反应条件
1: (i) NaNO2, aq. HCl, AcOH, (ii) SO3, aq. CuCl, AcOH, (iii) aq. NH3 2: CrO3, H2SO4 / acetic acid 3: aq. HCl / ethanol / Heating View Scheme
参考文献
Loynes,J.M. et al.
Journal of Medicinal Chemistry, 1965 , vol. 8, p. 691 - 694
