in acetonitrile (inert atm.); addn. of acetic chloride to soln. of rhenium compd. in CH3CN, stirring for 10 min, filtration, addn. of zinc compd., stirring for 30 min; filtration, evapn., sublimation at 40°C at 1E-1 mbar, GC and NMR;
参考文献
European Journal of Inorganic Chemistry, , # 25 p. 3929 - 3934
