2-二氮杂-1-苯乙酮合成路线 （共 259 条）
反应条件
2,5-dioxopyrrolidin-1-yl 3-(diphenylphosphanyl)propanoate in toluene T=0 - 23°C; chemoselective reaction;
参考文献
Raines, Ronald Thaddeus; Myers, Eddie Leonard
Patent: US2010/125132 A1, 2010 ;
Location in patent: Page/Page column 32 ;
反应条件
CaO in diethyl ether T=0°C; Arndt-Eistert synthesis; 3.08333 h;
参考文献
Pace, Vittorio; Verniest, Guido; Sinisterra, Josep-Vicent; Alcantara, Andres R.; De Kimpe, Norbert
Journal of Organic Chemistry, 2010 , vol. 75, # 16 p. 5760 - 5763
反应条件
1: in tetrahydrofuran; diethyl ether; acetonitrile T=20°C; P=5171.62 Torr; 0.416667 h; 2: With polymer-supported fluoride in tetrahydrofuran; diethyl ether; acetonitrile T=20°C; P=5171.62 Torr;
参考文献
Martin, Laetitia J.; Marzinzik, Andreas L.; Ley, Steven V.; Baxendale, Ian R.
Organic Letters, 2011 , vol. 13, # 2 p. 320 - 323
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in tetrahydrofuran T=0°C; 0.166667 h;
参考文献
Ideue, Eiji; Toma, Tatsuya; Shimokawa, Jun; Fukuyama, Tohru
Organic Syntheses, 2012 , vol. 89, p. 501 - 509
反应条件
aluminum oxide in diethyl ether; pentane
参考文献
Korneev; Richter
Synthesis, 1995 , # 10 p. 1248 - 1250
反应条件
Yield given. Multistep reaction;
参考文献
Chen, Zheng-Bo; Hong, Deng; Wang, Yan-Guang
Journal of Organic Chemistry, 2009 , vol. 74, # 2 p. 903 - 905
反应条件
C7H12N5O2S(1+)*CF3O3S(1-); triethylamine in neat (no solvent) T=20°C; Green chemistry;
参考文献
Muthyala, Manoj Kumar; Choudhary, Sunita; Kumar, Anil
Journal of Organic Chemistry, 2012 , vol. 77, # 19 p. 8787 - 8791
反应条件
aluminum oxide in diethyl ether; pentane
参考文献
Korneev; Richter
Synthesis, 1995 , # 10 p. 1248 - 1250
反应条件
1: benzoic acid With 2,4,6-trichloro-1,3,5-triazine; potassium carbonate in tetrahydrofuran; acetonitrile T=0°C; 2.75 h; 2: diazomethane in diethyl ether T=0 - 20°C; 12 h;
参考文献
Forbes; Barrett; Lewis; Smith
Tetrahedron Letters, 2000 , vol. 41, # 51 p. 9943 - 9947
反应条件
aluminum oxide in diethyl ether; pentane
参考文献
Korneev; Richter
Synthesis, 1995 , # 10 p. 1248 - 1250
