1-甲基-4-苯基乙炔苯合成路线 （共 165 条）
反应条件
silver fluoride; potassium hydrogencarbonate; bis(dibenzylideneacetone)-palladium(0) in acetonitrile T=20°C; Hiyama Coupling; 12 h;
参考文献
Tang, Jiansheng; Guo, Cancheng
Journal of Chemical Research, 2014 , vol. 38, # 2 p. 123 - 127
反应条件
C16H14N2O4Pd; silver(l) oxide in dichloromethane T=20°C; 12 h;
参考文献
Heo, Yumi; Kang, Yi Young; Palani, Thiruvengadam; Lee, Junseong; Lee, Sunwoo
Inorganic Chemistry Communications, 2012 , vol. 23, p. 1 - 5
反应条件
lanthanum; iodine in tetrahydrofuran T=67°C; Fritsch-Buttenberg-Wiechell rearrangement; 3 h; Inert atmosphere;
参考文献
Umeda, Rui; Yuasa, Takumi; Anahara, Namika; Nishiyama, Yutaka
Journal of Organometallic Chemistry, 2011 , vol. 696, # 9 p. 1916 - 1919
反应条件
palladium diacetate; triethylamine in N,N-dimethyl-formamide T=100°C; Sonogashira coupling; 12 h;
参考文献
Hwang, Lee Kyoung; Na, Youngim; Lee, Junseong; Do, Youngkyu; Chang, Sukbok
Angewandte Chemie - International Edition, 2005 , vol. 44, # 38 p. 6166 - 6169
反应条件
MCM-41-supported mercapto palladium(0) complex in water; N,N-dimethyl-formamide T=60°C; Stille coupling; 3 h;
参考文献
Zhao, Hong; Zheng, Guomin; Hao, Wenyan; Cai, Mingzhong
Applied Organometallic Chemistry, 2010 , vol. 24, # 2 p. 92 - 98
反应条件
copper(l) iodide; cesium fluoride in toluene; acetonitrile T=150°C; 0.5 h; Inert atmosphereMicrowave irradiation;
参考文献
Akubathini, Shashidhar Kumar; Biehl, Ed
Tetrahedron Letters, 2009 , vol. 50, # 16 p. 1809 - 1811
反应条件
tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran; ethylene glycol dimethyl ether; hexane T=80°C; Arylation; Suzuki-Miyaura cross-coupling reaction; 2 h;
参考文献
Castanet, Anne-Sophie; Colobert, Francoise; Schlama, Thierry
Organic Letters, 2000 , vol. 2, # 23 p. 3559 - 3561
反应条件
t-Bu2P(biphenyl); tetrabutyl ammonium fluoride; tris-(dibenzylideneacetone)dipalladium(0) in tetrahydrofuran T=20°C; 24 h;
参考文献
Faller, Jack W.; Kultyshev, Roman G.; Parr, Jonathan
Tetrahedron Letters, 2003 , vol. 44, # 3 p. 451 - 453
反应条件
tetrakis(triphenylphosphine) palladium(0); Cu(I) 3-methylsalicylate in ethylene glycol dimethyl ether T=40 - 45°C; inverse Sonogashira cross coupling reaction; 16 h; Inert atmosphere;
参考文献
Henke, Adam; Srogl, Jiri
Chemical Communications, 2010 , vol. 46, # 36 p. 6819 - 6821
反应条件
triethylamine T=100°C; Sonogashira Cross-Coupling; P=15201 Torr; 24 h; AutoclaveSchlenk technique; chemoselective reaction;
参考文献
Aronica, Laura Antonella; Caporusso, Anna Maria; Tuci, Giulia; Evangelisti, Claudio; Manzoli, Maela; Botavina, Maria; Martra, Gianmario
Applied Catalysis A: General, 2014 , vol. 480, p. 1 - 9
