1-甲基-4-苯基乙炔苯合成路线 （共 165 条）
反应条件
bis-triphenylphosphine-palladium(II) chloride; triethylamine; copper(l) chloride in acetonitrile T=80°C; Sonogashira Cross-Coupling; P=6080.41 Torr; 1 h; Autoclave; Concentration;
参考文献
Kim, Wonyoung; Park, Kyungho; Park, Ahbyeol; Choe, Juseok; Lee, Sunwoo
Organic Letters, 2013 , vol. 15, # 7 p. 1654 - 1657
反应条件
bis-(pyridin-2-yl)amine; Pd(NH3)2Cl2; triethylamine in water T=25°C; Sonogashira Cross-Coupling; 6 h; Inert atmosphere;
参考文献
Zhong, Hong; Wang, Jinyun; Li, Liuyi; Wang, Ruihu
Dalton Transactions, 2014 , vol. 43, # 5 p. 2098 - 2103
反应条件
norborn-2-ene; palladium diacetate; potassium acetate in N,N-dimethyl acetamide T=25°C; Cassar-Sonogashira reaction; 144 h;
参考文献
Motti, Elena; Rossetti, Manuela; Bocelli, Gabriele; Catellani, Marta
Journal of Organometallic Chemistry, 2004 , vol. 689, # 23 p. 3741 - 3749
反应条件
1: 1-(iodo)-4-methylbenzene; acetylenecarboxylic acid With 1-methyl-pyrrolidin-2-one; 1,1'-bis-(diphenylphosphino)ferrocene; tris-(dibenzylideneacetone)dipalladium(0); tetrabutyl ammonium fluoride T=20°C; Sonogashira coupling; 12 h; 2: bromobenzene T=90°C; 12 h;
参考文献
Moon, Jeongju; Jeong, Miso; Nam, Hyungoog; Ju, Jinhun; Moon, Joong Ho; Jung, Hyun Min; Lee, Sunwoo
Organic Letters, 2008 , vol. 10, # 5 p. 945 - 948
反应条件
triethylamine; gold(I) chloride; palladium dichloride in acetonitrile T=20°C; Sonogashira coupling;
参考文献
Panda, Biswajit; Sarkar, Tarun K.
Chemical Communications, 2010 , vol. 46, # 18 p. 3131 - 3133
反应条件
1: 4-methyl-chlorobenzene With diphenylphosphinoethane functionalized polystyrene resin-supported Pd(0) complex in N,N-dimethyl-formamide T=20°C; Stille Cross Coupling; 0.25 h; 2: 1-tributylstannyl-2-phenylacetylene in N,N-dimethyl-formamide T=120°C; Stille Cross Coupling; 11 h;
参考文献
Bahari, Siavash; Mohammadi-Aghdam, Babak; Molaei, Rahim; Gharibi, Zakiyeh
Canadian Journal of Chemistry, 2012 , vol. 90, # 9 p. 784 - 789
反应条件
sodium t-butanolate in benzene T=55°C; Sonogashira Cross-Coupling; 1 h;
参考文献
Scharf, Adam; Goldberg, Israel; Vigalok, Arkadi
Journal of the American Chemical Society, 2013 , vol. 135, # 3 p. 967 - 970
反应条件
sodium t-butanolate in benzene T=55°C; Sonogashira Cross-Coupling; 1 h;
参考文献
Scharf, Adam; Goldberg, Israel; Vigalok, Arkadi
Journal of the American Chemical Society, 2013 , vol. 135, # 3 p. 967 - 970
反应条件
bis-triphenylphosphine-palladium(II) chloride; triethylamine; copper(l) chloride in acetonitrile T=80°C; Sonogashira Cross-Coupling; P=6080.41 Torr; 1 h; Autoclave;
参考文献
Kim, Wonyoung; Park, Kyungho; Park, Ahbyeol; Choe, Juseok; Lee, Sunwoo
Organic Letters, 2013 , vol. 15, # 7 p. 1654 - 1657
反应条件
copper(l) iodide; palladium; triphenylphosphine; aluminum oxide; potassium fluoride Sonogashira coupling reaction; 0.0416667 h; microwave irradiation;
参考文献
Kabalka, George W.; Wang, Lei; Pagni, Richard M.
Tetrahedron, 2001 , vol. 57, # 38 p. 8017 - 8028
