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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
3-吡啶硼酸频哪醇酯
合成路线
（共 42 条）
56341-37-8
6-氯氧化吲哚
+
329214-79-1
3-吡啶硼酸频哪醇酯
→
反应条件
295800-01-0
反应条件
potassium phosphate; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl; tris-(dibenzylideneacetone)dipalladium(0) in butan-1-ol T=100°C; 1.65 h; Microwave irradiation;
参考文献
UNIVERSITY HEALTH NETWORK
Patent: WO2009/79767 A1, 2009 ;
Location in patent: Page/Page column 89 ;
WO 2009/079767 A1
626-55-1
3-溴吡啶
+
329214-79-1
3-吡啶硼酸频哪醇酯
→
反应条件
581-46-4
3,3'-联吡啶
反应条件
potassium carbonate; cyclopallated ferrocenylimine c in water; N,N-dimethyl-formamide T=110°C; Suzuki cross-coupling reaction; 5 h;
参考文献
Journal of Organometallic Chemistry, , vol. 691, # 6 p. 1301 - 1306
626-60-8
3-氯吡啶
+
329214-79-1
3-吡啶硼酸频哪醇酯
→
反应条件
581-46-4
3,3'-联吡啶
反应条件
caesium carbonate; cyclopallated ferrocenylimine c in water; N,N-dimethyl-formamide T=110°C; Suzuki cross-coupling reaction; 24 h;
参考文献
Journal of Organometallic Chemistry, , vol. 691, # 6 p. 1301 - 1306
→
反应条件
581-46-4
3,3'-联吡啶
+
794508-41-1
反应条件
potassium phosphate; palladium diacetate; tetra-(n-butyl)ammonium iodide; tri-cyclo-hexyl-phosphine in water; N,N-dimethyl-formamide T=90°C; Suzuki Coupling; Inert atmosphere;
参考文献
Organic Process Research and Development, , vol. 8, # 6 p. 955 - 957
109-09-1
2-氯吡啶
+
329214-79-1
3-吡啶硼酸频哪醇酯
→
反应条件
581-50-0
2,3'-联吡啶
反应条件
caesium carbonate; cyclopallated ferrocenylimine c in water; N,N-dimethyl-formamide T=110°C; Suzuki cross-coupling reaction; 24 h;
参考文献
Zhang, Jinli; Zhao, Liang; Song, Maoping; Mak, Thomas C.W.; Wu, Yangjie
Journal of Organometallic Chemistry, 2006 , vol. 691, # 6 p. 1301 - 1306
109-04-6
邻溴吡啶
+
329214-79-1
3-吡啶硼酸频哪醇酯
→
反应条件
581-50-0
2,3'-联吡啶
反应条件
potassium phosphate; (C5H5FeC5H3C(CH3)NC6H4CH3)PdCl(tricyclohexylphosphine); potassium acetate in 1,4-dioxane; water T=100°C; Suzuki coupling; 15 h; Inert atmosphere;
参考文献
Wang, Lianhui; Cui, Xiuling; Li, Jingya; Wu, Yusheng; Zhu, Zhiwu; Wu, Yangjie
European Journal of Organic Chemistry, 2012 , # 3 p. 595 - 603
576-22-7
2-溴-1,3-二甲苯
+
329214-79-1
3-吡啶硼酸频哪醇酯
→
反应条件
157402-43-2
反应条件
potassium carbonate; cyclopallated ferrocenylimine c in water; N,N-dimethyl-formamide T=110°C; Suzuki cross-coupling reaction; 10 h;
参考文献
Zhang, Jinli; Zhao, Liang; Song, Maoping; Mak, Thomas C.W.; Wu, Yangjie
Journal of Organometallic Chemistry, 2006 , vol. 691, # 6 p. 1301 - 1306
108-86-1
溴代苯
+
329214-79-1
3-吡啶硼酸频哪醇酯
→
反应条件
1008-88-4
3-苯基吡啶
反应条件
potassium carbonate; cyclopallated ferrocenylimine c in water; N,N-dimethyl-formamide T=110°C; Suzuki cross-coupling reaction; 6 h;
参考文献
Zhang, Jinli; Zhao, Liang; Song, Maoping; Mak, Thomas C.W.; Wu, Yangjie
Journal of Organometallic Chemistry, 2006 , vol. 691, # 6 p. 1301 - 1306
591-50-4
碘苯
+
329214-79-1
3-吡啶硼酸频哪醇酯
→
反应条件
1008-88-4
3-苯基吡啶
反应条件
potassium carbonate; cyclopallated ferrocenylimine c in water; N,N-dimethyl-formamide T=110°C; Suzuki cross-coupling reaction; 4 h;
参考文献
Zhang, Jinli; Zhao, Liang; Song, Maoping; Mak, Thomas C.W.; Wu, Yangjie
Journal of Organometallic Chemistry, 2006 , vol. 691, # 6 p. 1301 - 1306
108-90-7
氯苯
+
329214-79-1
3-吡啶硼酸频哪醇酯
→
反应条件
1008-88-4
3-苯基吡啶
反应条件
caesium carbonate; cyclopallated ferrocenylimine c in water; N,N-dimethyl-formamide T=110°C; Suzuki cross-coupling reaction; 24 h;
参考文献
Zhang, Jinli; Zhao, Liang; Song, Maoping; Mak, Thomas C.W.; Wu, Yangjie
Journal of Organometallic Chemistry, 2006 , vol. 691, # 6 p. 1301 - 1306
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