1,2,3,4-四氢吖啶合成路线 (共 54 条)
反应条件
1: 92 percent / p-Toluenesulfonic acid / benzene / Heating; Continuous removal of water 2: 42 percent / 750 °C / 0.01 Torr View Scheme
参考文献
Journal of Organic Chemistry, , vol. 45, # 8 p. 1547 - 1548
反应条件
hydrogen; palladium/alumina in decalin T=250°C; P=15200 Torr; Yield given. Yields of byproduct given;
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , p. 1769 - 1774
反应条件
in cyclohexane 2.5 h; Irradiation;
参考文献
Olsen
Tetrahedron Letters, 1991 , vol. 32, # 39 p. 5235 - 5238
反应条件
hydrogen; Pt/Al2O3 in decalin T=149.9°C; P=52504.2 Torr; 0.166667 h; effect of time; Product distribution;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 62, # 12 p. 3994 - 4001
反应条件
sulfuric acid in methanol 2.5 h; Irradiation;
参考文献
Olsen
Tetrahedron Letters, 1991 , vol. 32, # 39 p. 5235 - 5238
反应条件
1: Pb(OCOCH3)4 2: ZnBr2 / CHCl3 / 2 h / 90 - 100 °C / other 1,2,3-benzotriazine, other enamines of karbonyl compounds View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 46, # 2 p. 332 - 334
反应条件
[RuH2(η2-H2)2(PCy3)2]; hydrogen in cyclohexane T=80°C; P=2250.23 Torr; 1 h; Catalytic behavior;
参考文献
Borowski, Andrzej F.; Vendier, Laure; Sabo-Etienne, Sylviane; Rozycka-Sokolowska, Ewa; Gaudyn, Alicja V.
Dalton Transactions, 2012 , vol. 41, # 46 p. 14117 - 14125
反应条件
[RuH2(η2-H2)2(PCy3)2]; hydrogen in cyclohexane T=80°C; P=2250.23 Torr; 1 h; Catalytic behavior;
参考文献
Dalton Transactions, , vol. 41, # 46 p. 14117 - 14125
反应条件
phosphorus pentoxide
参考文献
Journal and Proceedings of the Royal Society of New South Wales, , vol. 83, p. 117
反应条件
zinc dibromide in chloroform T=90 - 100°C; 2 h; Yield given;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 46, # 2 p. 332 - 334