N,N'-二环己基草酰胺合成路线 （共 19 条）
反应条件
(cis,trans)-1,4-dichlorobut-2-ene; Pd2(PPh3)2Cl2 in tetrahydrofuran T=20°C; P=38000 Torr; 17 h;
参考文献
Hiwatari, Kozo; Kayaki, Yoshihito; Okita, Koshi; Ukai, Tomohiro; Shimizu, Isao; Yamamoto, Akio
Bulletin of the Chemical Society of Japan, 2004 , vol. 77, # 12 p. 2237 - 2250
反应条件
(NH4)2S2O8; silver nitrate in hexane; water T=40°C; 3 h;
参考文献
Minisci, Francesco; Fontana, Francesca; Coppa, Fausta; Yan, Yong Ming
Journal of Organic Chemistry, 1995 , vol. 60, # 17 p. 5430 - 5433
反应条件
oxygen; anhydrous sulphate; palladium; zirconium oxide in acetonitrile T=135°C; P=30002.4 Torr; 1 h; Product distribution; Further Variations:CatalystsReaction partnersSolvents;
参考文献
Hoberg, Heinz; Fananas, F. Javier; Riegel, Hans Josef
Journal of Organometallic Chemistry, 1983 , vol. 254, # 2 p. 267 - 272
反应条件
oxygen; triphenylphosphine; AuCl(PPh3)2 T=200°C; P=37503.8 Torr; 3 h;
参考文献
Shi; Deng
Chemical Communications, 2001 , # 5 p. 443 - 444
反应条件
oxygen; anhydrous sulphate; zirconium oxide; palladium dichloride T=170°C; P=45003.6 Torr; 3 h; Title compound not separated from byproducts;
参考文献
Shi, Feng; Deng, Youquan; SiMa, Tianlong; Yang, Hongzhou
Journal of Catalysis, 2001 , vol. 203, # 2 p. 525 - 528
反应条件
oxygen; anhydrous sulphate; zirconium oxide; palladium dichloride T=170°C; P=45003.6 Torr; 3 h; Title compound not separated from byproducts;
参考文献
Shi, Feng; Deng, Youquan; SiMa, Tianlong; Yang, Hongzhou
Journal of Catalysis, 2001 , vol. 203, # 2 p. 525 - 528
反应条件
1: KOH / methanol / 15 °C 2: 24 percent / (NH4)2S2O8 / AgNO3 / hexane; H2O / 3 h / 40 °C View Scheme
参考文献
Minisci, Francesco; Fontana, Francesca; Coppa, Fausta; Yan, Yong Ming
Journal of Organic Chemistry, 1995 , vol. 60, # 17 p. 5430 - 5433
反应条件
1: pyridine / CH2Cl2 / 1 h / 0 °C 2: KOH / methanol / 15 °C 3: 24 percent / (NH4)2S2O8 / AgNO3 / hexane; H2O / 3 h / 40 °C View Scheme
参考文献
Milligan; Swan
Journal of the Chemical Society, 1959 , p. 2969,2976
反应条件
N'-(3-dimethylaminopropyl)-N-ethylcarbodiimide in N,N-dimethyl-formamide Condensation;
参考文献
Ohta, Shunsaku; Tsuno, Naoki; Maeda, Kazushi; Nakamura, Seikou; Taguchi, Norio; Yamashita, Masayuki; Kawasaki, Ikuo
Tetrahedron Letters, 2000 , vol. 41, # 23 p. 4623 - 4627
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; samarium diiodide in tetrahydrofuran T=65°C; 8 h; Title compound not separated from byproducts;
参考文献
Liu, Yun-Shan; Bei, Mei-Zhi; Zhou, Zhi-Hua; Takaki, Ken; Fujiwara, Yuzo
Chemistry Letters, 1992 , # 7 p. 1143 - 1144
