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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
碘代均三甲基苯二乙酸酯
合成路线
（共 23 条）
253185-03-4
+
33035-41-5
碘代均三甲基苯二乙酸酯
→
反应条件
3056-64-2
4-(1,1-二甲基乙基)苯酚乙酸盐
+
13189-51-0
反应条件
acridine acid; palladium diacetate in acetic anhydride; acetic acid T=100°C; 24 h; Reagent/catalyst; Overall yield = 68 percent; Overall yield = 146.2 mg;
参考文献
Cook, Amanda K.; Emmert, Marion H.; Sanford, Melanie S.
Organic Letters, 2013 , vol. 15, # 21 p. 5428 - 5431
33035-41-5
碘代均三甲基苯二乙酸酯
+
100-66-3
苯甲醚
→
反应条件
613-70-7
邻甲氧基苯乙酸酯
+
1200-06-2
4-甲氧基苯乙酸
+
5451-83-2
3-甲氧基苯基乙酸
反应条件
acridine acid; palladium diacetate in acetic anhydride; acetic acid T=100°C; 4 h; Reagent/catalyst; Overall yield = 61 percent; Overall yield = 113 mg;
参考文献
Cook, Amanda K.; Emmert, Marion H.; Sanford, Melanie S.
Organic Letters, 2013 , vol. 15, # 21 p. 5428 - 5431
253185-03-4
+
33035-41-5
碘代均三甲基苯二乙酸酯
→
反应条件
3056-64-2
4-(1,1-二甲基乙基)苯酚乙酸盐
+
13189-51-0
反应条件
acridine acid; palladium diacetate in acetic anhydride; acetic acid T=100°C; 24 h; Reagent/catalyst; Overall yield = 68 percent; Overall yield = 146.2 mg;
参考文献
Cook, Amanda K.; Emmert, Marion H.; Sanford, Melanie S.
Organic Letters, 2013 , vol. 15, # 21 p. 5428 - 5431
33035-41-5
碘代均三甲基苯二乙酸酯
+
71-43-2
苯
→
反应条件
122-79-2
乙酸苯酯
反应条件
acridine acid; palladium diacetate in acetic anhydride; acetic acid T=100°C; 5 h; Reagent/catalyst;
参考文献
Cook, Amanda K.; Emmert, Marion H.; Sanford, Melanie S.
Organic Letters, 2013 , vol. 15, # 21 p. 5428 - 5431
634-36-6
1,2,3-三甲氧基苯
+
33035-41-5
碘代均三甲基苯二乙酸酯
→
反应条件
17742-46-0
+
30225-80-0
反应条件
acridine acid; palladium diacetate in acetic anhydride; acetic acid T=100°C; 17 h; Reagent/catalyst; Overall yield = 38 percent; Overall yield = 97.4 mg;
参考文献
Cook, Amanda K.; Emmert, Marion H.; Sanford, Melanie S.
Organic Letters, 2013 , vol. 15, # 21 p. 5428 - 5431
33035-41-5
碘代均三甲基苯二乙酸酯
+
95-50-1
邻二氯苯
→
反应条件
17847-51-7
反应条件
acridine acid; palladium diacetate in acetic anhydride; acetic acid T=100°C; 24 h; Reagent/catalystConcentration;
参考文献
Cook, Amanda K.; Emmert, Marion H.; Sanford, Melanie S.
Organic Letters, 2013 , vol. 15, # 21 p. 5428 - 5431
91-20-3
萘
+
33035-41-5
碘代均三甲基苯二乙酸酯
→
反应条件
17847-51-7
+
61925-85-7
2,3-二氯苯酚乙酯
反应条件
acridine acid; palladium diacetate in acetic anhydride; acetic acid T=100°C; 17 h; Reagent/catalyst; Overall yield = 60 percent; Overall yield = 125 mg;
参考文献
Cook, Amanda K.; Emmert, Marion H.; Sanford, Melanie S.
Organic Letters, 2013 , vol. 15, # 21 p. 5428 - 5431
33035-41-5
碘代均三甲基苯二乙酸酯
+
108-90-7
氯苯
→
反应条件
876-27-7
乙酸-4-氯苯酯
+
13031-39-5
间氯苯乙酸乙酯
反应条件
acridine acid; palladium diacetate in acetic anhydride; acetic acid T=100°C; 16 h; Reagent/catalyst; Overall yield = 54 percent; Overall yield = 102.5 mg;
参考文献
Cook, Amanda K.; Emmert, Marion H.; Sanford, Melanie S.
Organic Letters, 2013 , vol. 15, # 21 p. 5428 - 5431
33035-41-5
碘代均三甲基苯二乙酸酯
+
100-66-3
苯甲醚
→
反应条件
613-70-7
邻甲氧基苯乙酸酯
+
1200-06-2
4-甲氧基苯乙酸
+
5451-83-2
3-甲氧基苯基乙酸
反应条件
acridine acid; palladium diacetate in acetic anhydride; acetic acid T=100°C; 4 h; Reagent/catalyst; Overall yield = 61 percent; Overall yield = 113 mg;
参考文献
Cook, Amanda K.; Emmert, Marion H.; Sanford, Melanie S.
Organic Letters, 2013 , vol. 15, # 21 p. 5428 - 5431
91-20-3
萘
+
33035-41-5
碘代均三甲基苯二乙酸酯
→
反应条件
17847-51-7
+
61925-85-7
2,3-二氯苯酚乙酯
反应条件
acridine acid; palladium diacetate in acetic anhydride; acetic acid T=100°C; 17 h; Reagent/catalyst; Overall yield = 60 percent; Overall yield = 125 mg;
参考文献
Cook, Amanda K.; Emmert, Marion H.; Sanford, Melanie S.
Organic Letters, 2013 , vol. 15, # 21 p. 5428 - 5431
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