硫代磷酸 S-(4-氯苯基) O,O-二甲基酯合成路线 (共 6 条)
反应条件
CsOH in dimethyl sulfoxide T=20°C; 20 h;
参考文献
Ouyang, Yue-Jun; Li, Yuan-Yuan; Li, Ning-Bo; Xu, Xin-Hua
Chinese Chemical Letters, 2013 , vol. 24, # 12 p. 1103 - 1105
反应条件
TeCl4; calcium carbonate in dichloromethane 1 h; -42 deg C, 5-10 min; room temp. 1 h;
参考文献
Watanabe; Inoue; Yamamoto; Ozaki
Synthesis, 1995 , # 10 p. 1243 - 1244
反应条件
triethylamine in acetonitrile T=-10°C;
参考文献
Barai, Hasi Rani; Lee, Hai Whang
Bulletin of the Korean Chemical Society, 2011 , vol. 32, # 7 p. 2339 - 2344
反应条件
1: chlorine / CH2Cl2 / 1 h 2: 27 g / CH2Cl2 / 0.75 h View Scheme
参考文献
Ye, Jing-Dong; Barth, Christofer D.; Anjaneyulu, Potluri S. R.; Tuschl, Thomas; Piccirilli, Joseph A.
Organic and Biomolecular Chemistry, 2007 , vol. 5, # 15 p. 2491 - 2497
反应条件
in dichloromethane 0.75 h;
参考文献
Ye, Jing-Dong; Barth, Christofer D.; Anjaneyulu, Potluri S. R.; Tuschl, Thomas; Piccirilli, Joseph A.
Organic and Biomolecular Chemistry, 2007 , vol. 5, # 15 p. 2491 - 2497
反应条件
(i) Cl2, (ii) /BRN= 956570/; Multistep reaction;
参考文献
Pilgram,K.; Korte,F.
Tetrahedron, 1965 , vol. 21, p. 1999 - 2013