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63148-62-9
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碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
331002-70-1
合成路线
（共 5 条）
1242840-80-7
+
1266374-59-7
→
反应条件
331002-70-1
反应条件
sodium acetate in acetic acid 2 h; Inert atmosphereReflux;
参考文献
Yu, Li-Fang; Li, Yuan-Yuan; Su, Ming-Bo; Zhang, Mei; Zhang, Wei; Zhang, Li-Na; Pang, Tao; Zhang, Run-Tao; Liu, Bing; Li, Jing-Ya; Li, Jia; Nan, Fa-Jun
ACS Medicinal Chemistry Letters, 2013 , vol. 4, # 5 p. 475 - 480
89-54-3
→
反应条件
331002-70-1
反应条件
1: ethanol / |Reflux; |Inert atmosphere 2: sodium acetate / acetic acid / 2 h / |Inert atmosphere; |Reflux View Scheme
参考文献
Yu, Li-Fang; Li, Yuan-Yuan; Su, Ming-Bo; Zhang, Mei; Zhang, Wei; Zhang, Li-Na; Pang, Tao; Zhang, Run-Tao; Liu, Bing; Li, Jing-Ya; Li, Jia; Nan, Fa-Jun
ACS Medicinal Chemistry Letters, 2013 , vol. 4, # 5 p. 475 - 480
6972-71-0
4,5-二甲基-2-硝基苯胺
→
反应条件
331002-70-1
反应条件
1: hydrogenchloride; sodium nitrite / water / 0.17 h / |Cooling with ice 2: borane dimethyl sulfide complex / tetrahydrofuran / 2.5 h / 50 - 60 °C / |Inert atmosphere 3: sodium acetate / acetic acid / 2 h / |Inert atmosphere; |Reflux View Scheme
参考文献
Yu, Li-Fang; Li, Yuan-Yuan; Su, Ming-Bo; Zhang, Mei; Zhang, Wei; Zhang, Li-Na; Pang, Tao; Zhang, Run-Tao; Liu, Bing; Li, Jing-Ya; Li, Jia; Nan, Fa-Jun
ACS Medicinal Chemistry Letters, 2013 , vol. 4, # 5 p. 475 - 480
88-14-2
糠酸
→
反应条件
331002-70-1
反应条件
1: hydrogenchloride; sodium nitrite / water / 0.17 h / |Cooling with ice 2: borane dimethyl sulfide complex / tetrahydrofuran / 2.5 h / 50 - 60 °C / |Inert atmosphere 3: sodium acetate / acetic acid / 2 h / |Inert atmosphere; |Reflux View Scheme
参考文献
Yu, Li-Fang; Li, Yuan-Yuan; Su, Ming-Bo; Zhang, Mei; Zhang, Wei; Zhang, Li-Na; Pang, Tao; Zhang, Run-Tao; Liu, Bing; Li, Jing-Ya; Li, Jia; Nan, Fa-Jun
ACS Medicinal Chemistry Letters, 2013 , vol. 4, # 5 p. 475 - 480
1270120-16-5
→
反应条件
331002-70-1
反应条件
1: borane dimethyl sulfide complex / tetrahydrofuran / 2.5 h / 50 - 60 °C / |Inert atmosphere 2: sodium acetate / acetic acid / 2 h / |Inert atmosphere; |Reflux View Scheme
参考文献
Yu, Li-Fang; Li, Yuan-Yuan; Su, Ming-Bo; Zhang, Mei; Zhang, Wei; Zhang, Li-Na; Pang, Tao; Zhang, Run-Tao; Liu, Bing; Li, Jing-Ya; Li, Jia; Nan, Fa-Jun
ACS Medicinal Chemistry Letters, 2013 , vol. 4, # 5 p. 475 - 480
