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乙二醇
甲醛
63148-62-9
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二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
1-苯乙基哌啶
合成路线
（共 36 条）
110-89-4
哌啶
+
292638-84-7
→
反应条件
332-14-9
1-苯乙基哌啶
反应条件
trifluorormethanesulfonic acid; 1,5-bis-(diphenylphosphino)-pentane; [Ru(η4-COD)(η3-methylallyl)2] in 1,4-dioxane T=100°C; 24 h;
参考文献
YALE UNIVERSITY
Patent: WO2005/77885 A1, 2005 ;
Location in patent: Page/Page column 20-21; 29-30 ;
110-89-4
哌啶
+
292638-84-7
→
反应条件
332-14-9
1-苯乙基哌啶
+
55606-20-7
反应条件
[Rh(COD)(DPEphos)][BF4] in toluene T=75°C; 72 h;
参考文献
Utsunomiya, Masaru; Kuwano, Ryoichi; Kawatsura, Motoi; Hartwig, John F.
Journal of the American Chemical Society, 2003 , vol. 125, # 19 p. 5608 - 5609
110-89-4
哌啶
+
122-78-1
苯乙醛
→
反应条件
332-14-9
1-苯乙基哌啶
反应条件
sodium tetrahydroborate
参考文献
Wichitnithad, Wisut; O'Callaghan, James P.; Miller, Diane B.; Train, Brian C.; Callery, Patrick S.
Bioorganic and Medicinal Chemistry, 2011 , vol. 19, # 24 p. 7482 - 7492
110-89-4
哌啶
+
60-12-8
苯乙醇
→
反应条件
332-14-9
1-苯乙基哌啶
反应条件
1,2-bis-(diphenylphosphino)ethane; palladium dichloride; lithium hydroxide hydrate in neat (no solvent) T=130°C; 24 h;
参考文献
Dang, Tuan Thanh; Ramalingam, Balamurugan; Shan, Siah Pei; Seayad, Abdul Majeed
ACS Catalysis, 2013 , vol. 3, # 11 p. 2536 - 2540
110-89-4
哌啶
+
50-00-0
甲醛
+
100-39-0
溴化苄
→
反应条件
332-14-9
1-苯乙基哌啶
反应条件
1: With trifluoroacetic acid; zinc in acetonitrile Mannich type reaction; 1 h; Inert atmosphere; 2: With ammonium chloride in water; acetonitrile
参考文献
Le Gall, Erwan; Haurena, Caroline; Sengmany, Stephane; Martens, Thierry; Troupel, Michel
Journal of Organic Chemistry, 2009 , vol. 74, # 20 p. 7971 - 7973
111-29-5
1,5-戊二醇
+
64-04-0
2-苯乙胺
→
反应条件
332-14-9
1-苯乙基哌啶
反应条件
ruthenium trichloride; tributylphosphine in 1,4-dioxane T=180°C; 5 h;
参考文献
Tsuji, Yasushi; Huh, Keun-Tae; Ohsugi, Yukihiro; Watanabe, Yoshihisa
Journal of Organic Chemistry, 1985 , vol. 50, # 9 p. 1365 - 1370
626-67-5
N-甲基哌啶
+
100-39-0
溴化苄
→
反应条件
332-14-9
1-苯乙基哌啶
反应条件
1: 1-methyl-piperidine With boron trifluoride diethyl etherate in tetrahydrofuran T=0°C; 0.166667 h; 2: With sec.-butyllithium in tetrahydrofuran T=-78°C; 1 h; 3: benzyl bromide With cesium fluoride in tetrahydrofuran T=-78 - -30°C; 1 h;
参考文献
Kessar; Singh
Synlett, 2001 , # 4 p. 517 - 518
100722-18-7
→
反应条件
332-14-9
1-苯乙基哌啶
反应条件
1,4-diaza-bicyclo[2.2.2]octane; Hg(II) trifluoroacetate; sodium cyanoborohydride in methanol 24 h; Ambient temperature;
参考文献
Sassaman, Mark B.
Tetrahedron, 1996 , vol. 52, # 33 p. 10835 - 10840
110-89-4
哌啶
+
292638-84-7
+
39166-25-1
→
反应条件
332-14-9
1-苯乙基哌啶
+
46346-12-7
反应条件
trifluorormethanesulfonic acid; [Ru(η4-COD)(η3-methylallyl)2]; 1,5-bis-(diphenylphosphino)-pentane in 1,4-dioxane T=100°C; 24 h; Product distribution / selectivity;
参考文献
YALE UNIVERSITY
Patent: WO2005/77885 A1, 2005 ;
Location in patent: Page/Page column 22-23; 34 ;
64-04-0
2-苯乙胺
+
142-29-0
环戊烯
→
反应条件
332-14-9
1-苯乙基哌啶
反应条件
1: cyclopentene With oxygen; ozone in methanol; dichloromethane T=-78°C; 2: phenethylamine With NaBH(OAc)3 in dichloromethane T=20°C; 2 h;
参考文献
Kyasa, Shivakumar; Fisher, Thomas J.; Dussault, Patrick H.
Synthesis, 2011 , # 21 art. no. M64811SS, p. 3475 - 3481
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