1-(2-甲基-1,3-二噻戊环-2-基)乙酮合成路线 （共 8 条）
反应条件
boron trifluoride diethyl etherate in dichloromethane T=25°C; 12 h;
参考文献
Barros; Barros, M. Teresa; Leitao; Leitao, Alcino J.; Maycock; Maycock, Christopher D.
Tetrahedron Letters, 1995 , vol. 36, # 36 p. 6537 - 6540
反应条件
water; toluene-4-sulfonic acid in acetone
参考文献
Fjeldskaar, Inger Reidun; Skatteboel, Lars
Acta Chemica Scandinavica, 1991 , vol. 45, # 4 p. 410 - 417
反应条件
water; toluene-4-sulfonic acid in acetone
参考文献
Fjeldskaar, Inger Reidun; Skatteboel, Lars
Acta Chemica Scandinavica, 1991 , vol. 45, # 4 p. 410 - 417
反应条件
water; 1-Fluoro-2,4,6-trimethylpyridinium trifluoromethanesulfonate in tetrahydrofuran; dichloromethane T=23°C;
参考文献
Kiselyov; Strekowski; Semenov
Tetrahedron, 1993 , vol. 49, # 11 p. 2151 - 2158
反应条件
1: 85 percent / Br2, Et3N / CCl4 / 10 h / Ambient temperature 2: 92 percent / H2O, p-toluenesulfonic acid / acetone View Scheme
参考文献
Fjeldskaar, Inger Reidun; Skatteboel, Lars
Acta Chemica Scandinavica, 1991 , vol. 45, # 4 p. 410 - 417
反应条件
mercury dichloride 24 h; Ambient temperature;
参考文献
Tanimoto, Shigeo; Jo, Shigeo; Sugimoto, Toyonari; Okano, Masaya
Bulletin of the Chemical Society of Japan, 1981 , vol. 54, # 10 p. 3237 - 3238
反应条件
1: 90 percent / baker's yeast; sucrose / H2O / 48 h / 23 °C / stirring 2: HN3 / DEAD; TPP / benzene / 72 h / 20 °C View Scheme
参考文献
Afonso; Barros; Godinho; Maycock
Synthesis, 1991 , # 7 p. 575 - 580
反应条件
n-butyllithium
1) hexane, THF, -78 deg C 2) 30 min, -78 deg C; Yield given. Multistep reaction;
参考文献
Doyle, Michael P.; Griffin, John H.; Chinn, Mitchell S.; Leusen, Daan van
Journal of Organic Chemistry, 1984 , vol. 49, # 11 p. 1917 - 1925
