anschliessend mit Aluminiumchlorid behandeln;

暂无反应条件数据

T=110 - 120°C;

T=180°C;

1: 96 percent / sodium borohydride / ethanol / 1.83 h / 55 - 60 °C 2: 93 percent / glacial acetic acid, conc. HCl / 0.25 h 3: 60 percent / 10percent palladium on charcoal / 300 - 305 °C View Scheme

1: 1.) hydrazine hydrate, 2.) KOH / 1.) triethylene glycol, 110 deg C, 60 min, 2.) 140 deg C, 2 h 2: 66 percent Chromat. / 2,3-dichloro-5,6-dicyano-1,4-benzoquinone (DDQ) / benzene / 5 h / Ambient temperature 3: 62 percent / iodine / benzene / 4 h / Heating 4: N-bromosuccinimid (NBS), benzoyl peroxide / CCl4 / 1.5 h / Heating 5: 1,5-diazabicyclo<4.3.0>non-5-ene (DBN) / tetrahydrofuran / 48 h / 5 °C 6: 92 percent / NaOMe / tetrahydrofuran; methanol / 0.25 h / 80 °C View Scheme

暂无反应条件数据

sodium tetrahydroborate in ethanol T=55 - 60°C; 1.83333 h;

isopropyl alcohol

potassium hydroxide; hydrazine hydrate 1.) triethylene glycol, 110 deg C, 60 min, 2.) 140 deg C, 2 h; Yield given. Multistep reaction;