1,1-二甲基哌啶-1-鎓碘化物合成路线 (共 12 条)
反应条件
in acetonitrile T=20°C;
参考文献
Maw, Graham; Thirsk, Carl; Whiting, Andrew
Tetrahedron Letters, 2001 , vol. 42, # 47 p. 8387 - 8390
反应条件
in dichloromethane T=20°C; 6 h;
参考文献
Voronkov; Tsyrendorzhieva; Rakhlin
Russian Journal of Organic Chemistry, 2010 , vol. 46, # 6 p. 794 - 797
反应条件
in diethyl ether Ambient temperature;
参考文献
Hilhorst, Ellen; Chen, Tjoe B. R. A.; Iskander, Atef S.; Pandit, Upendra K.
Tetrahedron, 1994 , vol. 50, # 26 p. 7837 - 7848
反应条件
in methanol; dichloromethane; N,N-dimethyl-formamide T=3°C; 72 h;
参考文献
Blade-Font, Artur; Rocabayera, Teodoro de Mas
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , p. 841 - 848
参考文献
Ladenburg
Justus Liebigs Annalen der Chemie, 1888 , vol. 247, p. 58
参考文献
Koehler
Archiv der Pharmazie (Weinheim, Germany), 1902 , vol. 240, p. 238
反应条件
1: 90 percent / CH2Cl2 / 140 h / Ambient temperature 2: 34 percent / methanol; dimethylformamide; CH2Cl2 / 72 h / 3 °C View Scheme
参考文献
Blade-Font, Artur; Rocabayera, Teodoro de Mas
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , p. 841 - 848
参考文献
Mueller et al.
Monatshefte fuer Chemie, 1953 , vol. 84, p. 1206,1216
参考文献
v. Braun; Kuehn; Goll
Chemische Berichte, 1926 , vol. 59, p. 2337
反应条件
cobalt(II) chloride; sodium sulfite; zinc in 1-methyl-pyrrolidin-2-one T=200°C; P=22502.3 Torr; 7 h; Autoclave;
参考文献
Lei, Yizhu; Zhang, Rui; Wu, Qing; Mei, Hui; Xiao, Bo; Li, Guangxing
Journal of Molecular Catalysis A: Chemical, 2014 , vol. 381, p. 120 - 125