4,5-二(苯基)-1-(苯基甲基)三唑合成路线 （共 9 条）
反应条件
(pentamethylCp)RuCl(PPh3)2 in benzene T=80°C; 2 h;
参考文献
Lo, Yih-Hsing; Wang, Tsang-Hsiu; Lee, Chia-Yi; Feng, Ying-Hsuan
Organometallics, 2012 , vol. 31, # 19 p. 6887 - 6899
反应条件
tetrakis(triphenylphosphine) palladium(0); silver(l) oxide in methanol T=60°C; Suzuki-Miyaura Coupling; 3 h; Inert atmosphere;
参考文献
Stefani, Helio A.; Silva, Nathalia C.S.; Vasconcelos, Stanley N.S.; Manarin, Flavia; Souza, Frederico B.
Tetrahedron Letters, 2013 , vol. 54, # 22 p. 2809 - 2812
反应条件
potassium hydroxide; bis-triphenylphosphine-palladium(II) chloride in tetrahydrofuran T=70°C; Suzuki coupling;
参考文献
Deng, Juan; Wu, Yong-Ming; Chen, Qing-Yun
Synthesis, 2005 , # 16 art. no. F06905SS, p. 2730 - 2738
反应条件
palladium diacetate; potassium carbonate; 1,3-bis(2,4,6-trimethylphenyl)imidazolinium chloride in N,N-dimethyl-formamide T=100°C; 12 h;
参考文献
He, Tao; Wang, Min; Li, Pinhua; Wang, Lei
Chinese Journal of Chemistry, 2012 , vol. 30, # 4 p. 979 - 984
反应条件
palladium diacetate; potassium carbonate; 1,3-bis(2,4,6-trimethylphenyl)imidazolinium chloride in N,N-dimethyl-formamide T=100°C; 12 h;
参考文献
He, Tao; Wang, Min; Li, Pinhua; Wang, Lei
Chinese Journal of Chemistry, 2012 , vol. 30, # 4 p. 979 - 984
反应条件
1: benzyl azide; 4,4,5,5-tetramethyl-2-(2-phenylethynyl)-[1,3,2]-dioxaborolane in 1,2-dichloro-benzene T=150°C; 24 h; Inert atmosphere; 2: iodobenzene With potassium phosphate; Pd2(dba)3; [(t-Bu)3PH]BF4 in 1,2-dichloro-benzene; acetonitrile T=50°C; 16 h; Inert atmosphere;
参考文献
Huang, Jianhui; Macdonald, Simon J.F.; Cooper, Anthony W.J.; Fisher, Gail; Harrity, Joseph P.A.
Tetrahedron Letters, 2009 , vol. 50, # 39 p. 5539 - 5541
反应条件
1.1: n-butyllithium / tetrahydrofuran / 0.67 h / -78 - 20 °C / |Inert atmosphere 1.2: 15 h / 20 °C / |Inert atmosphere 2.1: copper(l) iodide; N,N,N',N'',N''-pentamethyldiethylenetriamine / tetrahydrofuran / 20 °C / |Inert atmosphere 3.1: tetrakis(triphenylphosphine) palladium(0); silver(l) oxide / methanol / 3 h / 60 °C / |Inert atmosphere View Scheme
参考文献
Kavitha, Mitta; Mahipal, Bodugam; Mainkar, Prathama S.; Chandrasekhar, Srivari
Combinatorial Chemistry and High Throughput Screening, 2013 , vol. 16, # 8 p. 657 - 663
反应条件
1: copper(l) iodide; N,N,N',N'',N''-pentamethyldiethylenetriamine / tetrahydrofuran / 20 °C / |Inert atmosphere 2: tetrakis(triphenylphosphine) palladium(0); silver(l) oxide / methanol / 3 h / 60 °C / |Inert atmosphere View Scheme
参考文献
Kavitha, Mitta; Mahipal, Bodugam; Mainkar, Prathama S.; Chandrasekhar, Srivari
Combinatorial Chemistry and High Throughput Screening, 2013 , vol. 16, # 8 p. 657 - 663
反应条件
1: copper(l) iodide; N,N,N',N'',N''-pentamethyldiethylenetriamine / tetrahydrofuran / 20 °C / |Inert atmosphere 2: tetrakis(triphenylphosphine) palladium(0); silver(l) oxide / methanol / 3 h / 60 °C / |Inert atmosphere View Scheme
参考文献
Stefani, Helio A.; Silva, Nathalia C.S.; Vasconcelos, Stanley N.S.; Manarin, Flavia; Souza, Frederico B.
Tetrahedron Letters, 2013 , vol. 54, # 22 p. 2809 - 2812
