反应条件
1: 87 percent / CHCl3 / 5 h / Heating 2: 65 percent / AlCl3 / a) from 130 deg C to 140 deg C, 1 h, b) 80 deg C, 0.5 h 3: 90 percent / borane-dimethyl sulfide / toluene / a) 0 deg C, 15 min, b) reflux, 5 h 4: 86 percent / aq. NaHCO3 / 2 h / 20 - 50 °C View Scheme
参考文献
Benbrook, Doris M.; Madler, Matora M.; Spruce, Lyle W.; Birckbichler, Paul J.; Nelson, Eldon C.; Subramanian, Shankar; Mahika Weerasekare; Gale, Jonathan B.; Patterson Jr., Manford K.; Wang, Binghe; Wang, Wei; Lu, Shennan; Rowland, Tami C.; DiSivestro, Paul; Lindamood III, Charles; Hill, Donald L.; Berlin, K. Darrell
Journal of Medicinal Chemistry, 1997 , vol. 40, # 22 p. 3567 - 3583
