2-(2-氧代-2-苯乙基)-环己酮合成路线 （共 46 条）
反应条件
1: With sodium iodide in 1-methyl-pyrrolidin-2-one T=20°C; 11 h; 2: With water in 1-methyl-pyrrolidin-2-one 11 h; Product distribution / selectivity;
参考文献
GENKYO TEX
Patent: WO2008/116926 A1, 2008 ;
Location in patent: Page/Page column 48; 49 ;
WO 2008/116926 A1
反应条件
zinc(II) chloride in tetrahydrofuran T=40°C; Alkylation; 6 h;
参考文献
Yasuda, Makoto; Tsuji, Shoki; Shigeyoshi, Yusuke; Baba, Akio
Journal of the American Chemical Society, 2002 , vol. 124, # 25 p. 7440 - 7447
反应条件
zinc dibromide in tetrahydrofuran T=40°C; 2 h;
参考文献
Yasuda, Makoto; Tsuji, Shoki; Shigeyoshi, Yusuke; Baba, Akio
Journal of the American Chemical Society, 2002 , vol. 124, # 25 p. 7440 - 7447
反应条件
tris(n-butyl)phosphine oxide 1 h; Ambient temperature;
参考文献
Yasuda, Makoto; Katoh, Yasuhiro; Shibata, Ikuya; Baba, Akio; Matsuda, Haruo; Sonoda, Noboru
Journal of Organic Chemistry, 1994 , vol. 59, # 16 p. 4386 - 4392
反应条件
1: cyclohexanone With pyrrolidinium hydrochloride in water; N,N-dimethyl-formamide T=70°C; 2: styrene With manganese(IV) oxide; Cu(ClO4)2*6H2O in water; N,N-dimethyl-formamide T=70°C; 48 h;
参考文献
Xie, Jin; Huang, Zhi-Zhen
Chemical Communications, 2010 , vol. 46, # 11 p. 1947 - 1949
反应条件
tris(n-butyl)phosphine oxide in benzene T=25°C; 1 h;
参考文献
Yasuda, Makoto; Oh-hata, Tatsuhiro; Shibata, Ikuya; Baba, Akio; Matsuda, Haruo
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 7 p. 859 - 866
反应条件
in benzene T=80°C; 5 h;
参考文献
Yasuda, Makoto; Oh-hata, Tatsuhiro; Shibata, Ikuya; Baba, Akio; Matsuda, Haruo; Sonoda, Noboru
Bulletin of the Chemical Society of Japan, 1995 , vol. 68, # 4 p. 1180 - 1186
反应条件
1: With lithium boron tetrafluoride; [Ru(2,2′-bipyridine)3][hexafluorophosphate]2; 2,3,5,6-tetramethyl-p-benzoquinone in aceonitrile T=20°C; 12 h; Inert atmosphereIrradiationMolecular sieve; 2: With water; ammonium chloride in acetonitrile T=20°C; 1 h; Inert atmosphereMolecular sieve;
参考文献
Yasu, Yusuke; Koike, Takashi; Akita, Munetaka
Chemical Communications, 2012 , vol. 48, # 43 p. 5355 - 5357
反应条件
T=130°C; aza-Darzens reaction; 0.166667 h; Microwave irradiationneat (no solvent);
参考文献
Ma, Li-Jian; Inokuchi, Tsutomu
Chemical Communications, 2010 , vol. 46, # 37 p. 7037 - 7039
反应条件
tetrabutylammonium hexanitratocerate(IV); potassium carbonate in acetonitrile T=0°C; 2 h;
参考文献
Kohno, Yasushi; Narasaka, Koichi
Bulletin of the Chemical Society of Japan, 1995 , vol. 68, # 1 p. 322 - 329
