反应条件
dropwise addn. of the disilathiane to the tin chloride under Ar with stirring, stirring for 30 min at room temp., slow heating to 90°C; addn. of benzene to the residue, refluxing for 20 min with stirring, filtration, distn. of the benzene, grinding of the residue with pentane, filtration, recrystn. (ethanol), elem. anal.;
参考文献
Berwe, Hermann; Haas, Alois
Chemische Berichte, 1987 , vol. 120, p. 1175 - 1182
