反应条件
in dichloromethane
byproducts: (CH3)3SiF; trapping of MoF6 with dry ice/acetone (vac.), addn. of dry N2 or Ar, closing of system, warming, addn. of vapor into CH2Cl2 (yellow soln.), slow injection of hexamethyldisilthiane, stirring (cooling of react. vessel), backish-brown ppt.; filtration, washing with THF (soxhlet extractor), heating at 100°C (vac.); elem. anal.;
参考文献
Schleich; Chang; Barberio; Hanson
Journal of the Electrochemical Society, 1989 , vol. 136, # 11 p. 3274 - 3278