in benzene
byproducts: Me3SiCl; absence of air and moisture; simultaneous dropping of benzene solns. of equimolar amts. of Sn-compd. and S(SiMe3)2 into benzene, stirring (overnight, pptn.); filtration (after 10 days), washing (C6H6), sublimation (vac.);
参考文献
Jenkins, Linda S.; Wiley, Gerald R.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1979 , p. 1697 - 1700
Lebedev,E.P.; Baburina,V.A.
J. Gen. Chem. USSR (Engl. Transl.), 1975 , vol. 45, # 11 p. 2431 - 2434,2389 - 2391
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Fridland,D.V. et al.
J. Gen. Chem. USSR (Engl. Transl.), 1976 , vol. 46, # 2 p. 326 - 329,324 - 327