3-乙氧亚甲基-2,4-戊二酮合成路线 （共 53 条）
反应条件
in ethanol T=70°C; 1 h;
参考文献
Naito, Hiroyuki; Ohsuki, Satoru; Atsumi, Ryo; Minami, Megumi; Mochizuki, Mineko; Hirotani, Kenji; Kumazawa, Eiji; Ejima, Akio
Chemical and Pharmaceutical Bulletin, 2005 , vol. 53, # 2 p. 153 - 163
参考文献
Zhuo, Jin-Cong
Magnetic Resonance in Chemistry, 1997 , vol. 35, # 7 p. 432 - 440
反应条件
(i) piperidine, (ii) TsN3; Multistep reaction;
参考文献
Regitz,M.; Himbert,G.
Justus Liebigs Annalen der Chemie, 1970 , vol. 734, p. 70 - 85
反应条件
ozone in chloroform-d1 T=-70°C; 0.0833333 h;
参考文献
Helvetica Chimica Acta, , vol. 87, # 8 p. 2025 - 2049
反应条件
1: With ozone in dichloromethane T=-70°C; 0.416667 h; 2: With triphenylphosphine in dichloromethane T=0 - 20°C;
参考文献
Schank, Kurt; Beck, Horst; Pistorius, Susanne
Helvetica Chimica Acta, 2004 , vol. 87, # 8 p. 2025 - 2049
反应条件
1: 84 percent / ethanol / 24 h / Ambient temperature 2: 75 percent / aq. H2SO4 / 2 h / 50 °C 3: 70 percent / 6N hydrochloric acid / 10 h / Heating View Scheme
参考文献
Journal of Heterocyclic Chemistry, , vol. 22, p. 1503 - 1509
反应条件
ethanol; sodium ethanolate
参考文献
Graham et al.
Journal of the American Chemical Society, 1945 , vol. 67, p. 1294
反应条件
1: 84 percent / ethanol / 24 h / Ambient temperature 2: 75 percent / aq. H2SO4 / 2 h / 50 °C View Scheme
参考文献
Mosti, Luisa; Schenone, Pietro; Menozzi, Giulia
Journal of Heterocyclic Chemistry, 1985 , vol. 22, p. 1503 - 1509
反应条件
in ethanol 24 h; Ambient temperature;
参考文献
Mosti, Luisa; Schenone, Pietro; Menozzi, Giulia
Journal of Heterocyclic Chemistry, 1985 , vol. 22, p. 1503 - 1509
参考文献
Claisen
Justus Liebigs Annalen der Chemie, 1897 , vol. 297, p. 57
Chemische Berichte, 1893 , vol. 26, p. 2731
