oxalyl dichloride; Ph3PCl(+)Cl(-) in chloroform T=20°C; Appel reaction; 7 h;
参考文献
Denton, Ross M.; An, Jie; Adeniran, Beatrice; Blake, Alexander J.; Lewis, William; Poulton, Andrew M.
Journal of Organic Chemistry, 2011 , vol. 76, # 16 p. 6749 - 6767
Smith, Keith; Pollaud, Guy M
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1994 , # 24 p. 3519 - 3520
oxalyl dichloride; Ph3PCl(+)Cl(-) in chloroform T=20°C; Appel reaction; 7 h;
参考文献
Denton, Ross M.; An, Jie; Adeniran, Beatrice; Blake, Alexander J.; Lewis, William; Poulton, Andrew M.
Journal of Organic Chemistry, 2011 , vol. 76, # 16 p. 6749 - 6767
titanium(IV) isopropylate; tert.-butylhydroperoxide; L-(+)-diisopropyl tartrate; MS 4 Angstroem in 2,2,4-trimethylpentane; dichloromethane T=-20°C; Sharpless asymmetric epoxidation; 5 h; Title compound not separated from byproducts;
参考文献
Wang, Hao; Kozekov, Ivan D.; Harris, Thomas M.; Rizzo, Carmelo J.
Journal of the American Chemical Society, 2003 , vol. 125, # 19 p. 5687 - 5700