反应条件
1: 5-Bromo-1H-indole With potassium hydride in tetrahydrofuran; mineral oil T=0°C; 1 h; Inert atmosphere; 2: With tert.-butyl lithium in tetrahydrofuran; mineral oil; pentane T=-78°C; 0.25 h; Inert atmosphere; 3: N-(trifluoroacetyl)piperidine in tetrahydrofuran; mineral oil; pentane T=-78°C; 2 h; Inert atmosphere;
参考文献
Murai, Yuta; Sakihama, Yasuko; Hashidoko, Yasuyuki; Hashimoto, Makoto; Hatanaka, Yasumaru; Masuda, Katsuyoshi
Journal of Organic Chemistry, 2012 , vol. 77, # 19 p. 8581 - 8587,7
Title/Abstract Full Text Show Details
Murai, Yuta; Masuda, Katsuyoshi; Sakihama, Yasuko; Hashidoko, Yasuyuki; Hatanaka, Yasumaru; Hashimoto, Makoto
Journal of Organic Chemistry, 2012 , vol. 77, # 19 p. 8581 - 8587