sodium perchlorate in water NH2Cl soln. was added to cation-exchange column in H(1+) form (acidified with 3 M HCl, equilibrated with 0.1 M HClO4 and 0.1 M NaClO4, rinsed with water until neutral pH), eluted with water; monitored spectrophotometrically;
参考文献
Hand, Vincent C.; Margerum, Dale W.
Inorganic Chemistry, 1983 , vol. 22, p. 1449 - 1456
in water Kinetics; byproducts: OH(1-); reaction of excess sulfite with NCl3 in acetate buffer (25°C, pH 3.8-4.6); study by pulsed-accelerated-flow spectrophotometer (PAF);
参考文献
Yiin, Boudin S.; Margerum, Dale W.
Inorganic Chemistry, 1990 , vol. 29, p. 1942 - 1948